Preparation method and application for fructus gardeniae extract for tobacco

An extract, the technology of gardenia smoke, applied in the field of preparation of gardenia smoke extract, can solve the problems of reducing the pH value of smoke, achieve the effects of improving aroma quality, high product yield, and reducing irritation

Active Publication Date: 2016-11-23
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Using gardenia fruit as the raw material for aroma, compound enzyme hydrolysis, multiple solvent low-temperature extraction and molecular distillation refining technology are used to prepare gardenia extract for tobacco and apply it in reconstituted tobacco leaves to make its appearance and color more natural and even, close to high-quality Tobacco leaves, and coordinate with the smoke, reduce the pH value of the smoke, enrich the aroma, reduce irritation and miscellaneous gas, and improve the taste, which has not been reported yet

Method used

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  • Preparation method and application for fructus gardeniae extract for tobacco
  • Preparation method and application for fructus gardeniae extract for tobacco

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] A preparation method of the extract of Gardenia jasminoides:

[0022] 1) Put the gardenia fruit into an extraction tank after being crushed, add water with a mass ratio of 1:20, and add lactic acid bacteria and compound enzymes in an amount of 0.3% of the gardenia fruit mass, stir evenly, and dissolve at 45°C and pH Under natural conditions, ferment for 3 hours to obtain a gardenia fermented liquid;

[0023] Described lactic acid bacteria and compound enzyme are: account for 0.3% of gardenia fruit quality altogether, wherein lactic acid bacteria freeze-dried bacteria powder (food grade) accounts for 0.15%, β-glucosidase (food grade, enzyme activity is 1000u / g) accounts for 0.075% %, neutral protease (food grade, enzyme activity 50,000 u / g) accounts for 0.075%;

[0024] 2) Alcohol precipitation and purification: add 15% ethanol (95%, food grade) of water volume to the gardenia fruit fermentation broth, extract 3 times at low temperature and pressure, filter with suction...

Embodiment 2

[0029] A preparation method of an extract of gardenia jasminoides for tobacco use, comprising the following steps:

[0030] 1) Put the gardenia fruit into an extraction tank after being crushed, add water with a mass ratio of 1:30, and add lactic acid bacteria and compound enzymes according to 0.18% of the gardenia fruit mass, stir evenly, and put it under natural conditions of 50°C and pH , fermented for 4h to obtain gardenia fermented liquid;

[0031] Described lactic acid bacteria and compound enzyme are: account for 0.18% of gardenia fruit quality altogether, wherein lactic acid bacteria freeze-dried bacterial powder (food grade) accounts for 0.1%, β-glucosidase (food grade, enzyme activity is 10,000 u / g) Accounted for 0.05%, neutral protease (food grade, enzyme activity 120,000 u / g) accounted for 0.03%;

[0032] 2) Alcohol precipitation and purification: add 25% ethanol (food grade, 95%) of water volume to the gardenia fruit fermentation liquid, extract 3 times at low te...

Embodiment 3

[0037] A preparation method of an extract of gardenia jasminoides for tobacco use, comprising the following steps:

[0038] 1) Put the gardenia fruit into an extraction tank after being crushed, add water with a mass ratio of 1:40, and add lactic acid bacteria and compound enzymes according to 0.25% of the gardenia fruit mass, stir evenly, and store at 60°C and pH natural conditions , fermented for 6h to obtain gardenia fruit fermentation liquid;

[0039] Described lactic acid bacteria and compound enzyme are: account for 0.25% of gardenia fruit quality altogether, wherein lactic acid bacteria freeze-dried bacteria powder (food grade) accounts for 0.14%, β-glucosidase (food grade, enzyme activity is 9000u / g) accounts for 0.07% %, neutral protease (food grade, enzyme activity 200,000 u / g) accounts for 0.04%;

[0040] 2) Alcohol precipitation and purification: add 30% ethanol (food grade, 95%) of water volume to the gardenia fruit fermentation liquid, extract 3 times at low tem...

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Abstract

The invention discloses a preparation method for a fructus gardeniae extract for tobacco. The preparation method is characterized by comprising the following steps: (1) crushing fructus gardeniae fruits, adding the crushed fructus gardeniae fruits into an extracting tank, adding water, and adding lactobacilli and complex enzyme for fermenting to obtain fructus gardeniae fruit fermentation liquid, wherein the fructus gardeniae fruit and the water are in the mass ratio of 1 : (20 to 40); (2) performing alcohol precipitation and purification on the fructus gardeniae fruit fermentation liquid to obtain secondary fructus gardeniae concentrated liquid; (3) performing molecular distillation refining, namely, performing vacuum concentrating on the secondary fructus gardeniae concentrated liquid to obtain tertiary fructus gardeniae concentrated liquid, adding propylene glycol, performing further separation and purification on the tertiary fructus gardeniae concentrated liquid in molecule distillation equipment, collecting a light component, performing molecular distillation purifying on a heavy component again, and combining two light components to obtain the fructus gardeniae extract for the tobacco. According to the preparation method, the fructus gardeniae extract for the tobacco is prepared by adopting compound fermenting, solvent low-temperature extracting and molecular distillation refining, and is applied to reconstituted tobacco, so that the appearance colour and lustre of the reconstituted tobacco are more natural and uniform, and are close to those of high-quality tobacco; the pH value of smoke is reduced; aroma is enriched; stimulation and miscellaneous gas are reduced; the smoking taste is improved.

Description

technical field [0001] The invention relates to the technical field of tobacco additives, in particular to a preparation method and application of a gardenia tobacco extract. Background technique [0002] Reconstituted tobacco leaves are mainly composed of tobacco powder, chips, tobacco stems or low-grade tobacco leaves with adhesives and other additives. However, there are also taste defects such as heavy miscellaneous gas, strong irritation and unpleasant taste, which affect the use effect and addition amount of reconstituted tobacco leaves in cigarette products. The usual practice in China is to use additives to improve. At present, the most used additives are tobacco and natural plant extracts. These extracts are generally obtained through water, alcohol extraction or molecular distillation. The degree of improvement in cigarette quality after adding Limited, there are still defects such as large irritation and a lot of miscellaneous gas. [0003] Gardenia (scientific ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/26A24B15/28A24F47/00
CPCA24B15/26A24B15/28A24F47/004
Inventor 魏敏姚元军陈义坤罗诚浩高颂李冉刘志昌宋旭艳潘曦
Owner HUBEI CHINA TOBACCO IND
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