394results about How to "Soluble in water" patented technology

The invention relates to an amphoteric ionic polymer clay stabilizer and a preparation method thereof. The polymer has water solubility, is low in use level and shows excellent temperature resistance and shear resistance. According to the technical scheme, the amphoteric ionic polymer clay stabilizer is prepared from the following raw materials and monomers in percentage by mass: 53.5-59.9 percent of acrylamide AM; 40-45 percent of sodium acrylate NaAA (obtained from neutralization of crylic acid and sodium hydroxide), 0.1-1.5 percent of N-allyl oleamide NAO and 0.1-1.5 percent of dimethyl diallyl ammonium chloride DMDAAC. The preparation method comprises the following steps: firstly adding NAO in a reactor, then adding an emulsifier and water; after complete emulsification, adding AM, NaAA, DMDAAC to prepare a solution with the total mass percentage concentration of monomer being 10-25 percent, adjusting pH to be 6-8, and introducing N2 for 20 min; then adding an initiator, continuing to introduce N2 for 20 min, and reacting for 8-12 h at 30-70 DEG C; washing with absolute ethyl alcohol, grinding and drying to obtain AM/NaAA/DMDAAC/NAO quadripolymer. The result of an anti-swelling test of 0.2wt% solution shows that the anti-swelling rate can reach 86 percent.

The invention belongs to the field of super-amphiphobic materials and discloses water-borne epoxy resin and a super-amphiphobic coat as well as a preparation method and application of the water-borne epoxy resin and the super-amphiphobic coat. The water-borne epoxy resin is a polymer with the structural formula of P (A-r-B) and is obtained through the polymerization reaction of a water-soluble monomer A and a monomer B, wherein the mass ratio of A and B is 1: (0.2-20), and the tail end of the monomer B is an epoxy group. The obtained water-borne epoxy resin is dissolved into solvent, then a fluorine-containing substance, particles and a catalyst are added to the solvent to obtain a mixed solution; the mixed solution is stirred for reaction, and distilled water is dropwise added to form a water solution; a base material is soaked in the water solution, or the water solution is sprayed on the surface of the base material, and the super-amphiphobic coat is formed on the surface of the base material after drying treatment. The super-amphiphobic coat is simple to construct and has excellent lyophobic and oleophobic properties and excellent durability.

Water-dilutable brushing paints based on water-soluble alkyd resins rendered water-soluble through neutralization of methacrylic acid groups thereon are described. The brushing paints have favorable applicational properties, especially with regard to wet-edge time and brushability.

Colored detergent bars are provided comprising water soluble polymeric colorants that exhibit excellent non-staining performance on fabrics and other contacted surfaces, including manufacturing and/or washing equipment, are easy to process into the desired detergent bar compositions, and do not exhibit any appreciable harmful effects to the environment. The particular polymeric colorants utilized in this respect are of very high molecular weight (in order to assure staining will not occur on target cleaning surfaces), are extremely water soluble, provide excellent vivid and aesthetically pleasing color shades within the target bar compositions, and are present as liquid or waxy pastes at room and at processing temperatures. The ultimate laundry bar product thus exhibits highly pleasing colors for product distinction as well as for aesthetic purposes.

Provided is preparation of a water-soluble luminous silver nano cluster with double-stranded DNA as a template. Firstly, single-stranded DNA rich in cytosine base group is used, 6 cytosine base group loops are reserved in the single-stranded DNA, the total number of the cytosine base groups is 29, single-stranded DNA rich in guanine base group complements the single-stranded DNA and is added, the total number of the guanine base groups is 23, the double-stranded DNA with the 6 cytosine base group loops is formed through the annealing function and is used as the template, and synthesis is achieved through the method of adding sodium borohydride to restore silver nitrate. The preparation process is simple, easy to implement and environmentally friendly, and the preparation can be applied to the preparation of other luminous nano materials. In addition, new nano materials synthesized through the method have water solubility, a high quantum yield, light stability, good biocompatibility and other performance, and have potential wide application to the fields of biosensors, cell imaging, clinical medicine and the like.

The invention belongs to the field of biological engineering and relates to chitosan modification. The chitosan modification comprises the following steps of: adding protein or polypeptide; adding transglutaminase; adjusting the pH value; removing precipitates after full reaction; and desalting and drying for modification. The modified chitosan produced by the technical scheme disclosed by the invention is good in water solubility, does not generate precipitate at the pH value of 3-10, and is small in viscosity. Moreover, the functions including strong adsorption, antibacterial property and the like of the chitosan are kept, and the application prospect is extensive.

The invention discloses an aqueous finish paint used for coiled material. For a present aqueous paint used for steel band, in the preparation of epoxy modified polyester resin in the paint, it becomes aqueous must after amine neutralization, thereby, the steel band coated by the paint has the disadvantage of poor coating film water resistance. The aqueous finish painting in the invention comprises the following components: water soluble saturated polyester resin 45-50%, pigment 25-35%, aqueous defoaming agent 0.2-0.5%, aqueous wetting and dispersing agent 0.5-0.8%, aqueous leveling agent 0.3-1.0%, ethers solvent 2-5%, water 5-10%, water soluble amino resin 5-8%baking vanish cooling catalyst 0.2-0.8%, delustering powder 0-1.0% and aqueous anti-scratch agent 0-0.1%. The invention realizes water solubility of polyester resin by dicarboxybenzenesulfonic acid sodium salt, does not need amine neutralization, and achieves coating film with good water resistance.

A method of preparing a high purity metal nitride and/or oxide powder is provided, comprising: heating a metal salt and an organic fuel to an ignition temperature in a nitrogen-rich atmosphere, forming a first composition; and optionally heating the first composition to a heat treatment temperature, which heat treatment temperature is above the ignition temperature and below 1000° C., in a nitrogen-rich atmosphere until the metal nitride and/or oxide powder is formed.

The invention relates to a ferric fluorescent probe compound as well as a preparation method and application thereof. The ferric fluorescent probe compound has the structure in formula I in the specification. The preparation method comprises the following steps: mixing rhodamine B with anhydrous ethanediamine and refluxing in ethyl alcohol to prepare amide of rhodamine; protecting hydroxyl of binaphthol by chloromethyl methyl ether, reacting with N,N-dimethylformamide under the action of butyl lithium, and removing methyl of methyl ether by hydrochloric acid to obtain binaphthol with aldehyde group; finally refluxing the amide of rhodamine and the binaphthol with aldehyde group in ethyl alcohol and washing to obtain the pure ferric fluorescent probe compound. The probe compound has favorable selectivity and sensitivity for the ferric ions, is simple to treat before sample detection and free of causing toxicity to cells, and is used for detecting the ferric ions in the water environment or the biological cells.

The invention relates to an ellagic acid supramolecular combination and a preparation method. The substance is an anti-oxidant and has the anti-cancer effect, and the ellagic acid supramolecular combination belongs to the technical field of drugs and health care products. The ellagic acid supramolecular combination is composed of raw materials according to the following weight ratio that ellagic acid: cyclodextrin: emulsifier is equal to 1: (1-50): (0-10). The ellagic acid, the cyclodextrin and the emulsifier are added into a colloid mill, and the ellagic acid supramolecular combination is prepared by grinding and drying. The combination has the advantages of higher solubility, high dissolution rate, good stability and higher relative bioavailability.

In one embodiment, the present application discloses powder and aqueous formulations comprising a stabilized, aqueous purified cannabis oil emulsion comprising: a) CBD and THC wherein the ratio of CBD:THC by wt/wt is from 1,050:1 to 1:1,050, and b) at least one emulsifier selected from the group consisting of Poloxamer 188, Polysorbate 80, Polysorbate 20, Vit E-TPGS (TPGS), TPGS-1000, TPGS-750-M, Solutol HS 15, PEG-40 hydrogenated castor oil, PEG-35 Castor oil, PEG-8-glyceryl capylate/caprate, PEG-32-glyceryl laurate, PEG-32-glyceryl palmitostearate, Polysorbate 85, polyglyceryl-6-dioleate, sorbitan monooleate, Capmul MCM, Maisine 35-1, glyceryl monooleate, glyceryl monolinoleate, PEG-6-glyceryl oleate, PEG-6-glyceryl linoleate, oleic acid, linoleic acid, propylene glycol monocaprylate, propylene glycol monolaurate, polyglyceryl-3 dioleate, polyglyceryl-3 diisostearate and lecithin with and without bile salts, and mixtures thereof; and the uses in the treatment of diseases.

The invention discloses polyethylene glycol-chitosan self-assembled nanoparticles and a preparation method thereof, belonging to the technical field of preparation of a functional material. Chitosan derivative with water solubility and biocompatibility is obtained by modifying chitosan by polyethylene glycol, so as to prepare the polyethylene glycol-chitosan self-assembled nanoparticles. The polyethylene glycol-chitosan self-assembled nanoparticles have the advantages that TEMED (tetramethylethylenediamine).HCL is taken as a diluent; EDC (dichloroethane) and NHS are taken as activating agents under a mild condition; the polyethylene glycol chitosan derivative with water solubility and biocompatibility is prepared by grafting mPEG-COOH on CS in a covalent coupling manner and modifying the chitosan by PEG (polyethylene glycol), so that the nanoparticles can be formed in a water solution in a self-assembling manner.

The invention belongs to the technical field of coating and discloses water-based organic silicon fluorine modified graphene oxide/epoxy resin coating and a preparation method thereof. The coating comprises a component A and a component B, wherein the component A comprises 30 to 70 parts by weight of epoxy resin, 20 to 80 parts by weight of hydrophilic polyether-containing modified epoxy resin and30 to 70 parts by weight of water; the component B comprises 10 to 40 parts by weight of a water-based epoxy curing agent, 0.1 to 10 parts by weight of organic silicon fluorine modified graphene oxide, 1 to 10 parts by weight of imvite, 1 to 5 parts by weight of zinc phosphate, 20 to 70 parts by weight of water, 0.3 to 2 parts by weight of a dispersing agent, 0.3 to 2 parts by weight of a defoaming agent, 0.3 to 2 parts by weight of a wetting agent and 0.3 to 2 parts by weight of a leveling agent; the weight ratio of the component A to the component B is 100:(40-60). The coating formed by thecoating provided by the invention has high hardness, water tolerance, acid and alkali resistance, ageing resistance, solvent resistance, salt tolerance, salt spray resistance and the like, and has high corrosion resistance.

The invention discloses a preparation method of water-soluble luminescent quantum dots for fingerprint appearance, belonging to the field of biomarkers. The chemical composition of the water-soluble luminescent quantum dots is InP/ZnS. The preparation method comprises the following steps: under the inert atmosphere, weighing and adding an indium source, a phosphorus source, a surface active agent and a methylbenzene solvent of proper amount at certain stoichiometric ratio into a reactor, wherein the heating temperature is 150-200 DEG C, reacting for 18-36 hours to obtain gray black solution; using methyl alcohol to clean for a plurality of times; putting products in a vacuum drying box at certain temperature, drying for 8-12 hours to obtain solid powder of InP; dissloving a certain amount of solid powder into an organic solvent, adding alkaline solution (pH is 7.5-10.5) containing mercaptoacetic acid and zinc ions, stirring for a period of time at the temperature of 40-60 DEG C; removing an upper organic layer and obtaining lower-layer water-phase solution; and taking a certain amount of solution, adding the alkaline solution containing the mercaptoacetic acid and the zinc ions, stirring for 0.5-1.5 hours under the irradiation of ultraviolet light and obtaining water-soluble InP/ZnS end products.

The invention discloses a preparation method of a water dispersible nano copper cooling lubricant for cold rolling. In the lubricant, oleate is used as a surfactant, divalent copper salt is used as a copper element, and hydrazine hydrate is used as a reducing agent. Nano copper is selected as a main raw material of the lubricant, and meanwhile, certain dispersant and surfactant are added to prepare the water dispersible nano copper cooling lubricant applicable to a cold rolling process. The invention aims at improving the lubricity of cold rolling, a friction surface can be primed and repaired to a certain extent through products of a friction chemical reaction, and thus, rolled steel has self repairing action.

Liquid organic fertilizer comprises the following ingredients: 19% of soluble nitrogen-phosphorus-potassium raw material, 30% of humic acid agent, 20% of alginic acid agent, 10% of amino acid agent, 10% of fulvic acid potassium agent, 5% of soil conditioner and 6% of chelated medium trace element agent. The liquid organic fertilizer has the benefits that the liquid organic fertilizer can quickly supplement soil nutrition, allows a plant root system to be capable of directly absorbing organic matter and chelated medium trace elements, improves crop quality, avoids physiological diseases of crops, is green and safe, achieves agricultural production and income increase, is convenient to use and pollution-free, has good prevention and treatment effects on continuous cropping diseases and soil-borne diseases, breaks soil hardening, improves a soil microorganism ecological environment, increases the organic matter, fixes nitrogen, dissolves phosphorus and potassium, reduces the usage amount of inorganic fertilizer and protects the environment.

The invention relates to an amino functional polysiloxane with formulas III and IV, a preparation method thereof and the use as a binder, and the composite based on the amino functional polysiloxane, in particular to the stable chloride-free composite of polysiloxane acidic salt and the preparation and use thereof. The R<1> and R<2> are independent and are respectively expressed by R<1> as -(CH2) pAr<1>, -(CH) pAr<1>, -(CH) pAr<1>-(CHCH2) or -(CH2) pAr<1>-(CHCH2) and/or R<2> as -(CH2) qAr<2>, -(CH) pAr<2>, -(CH) pAr<2>-(CHCH2) or -(CH2) pAr<2>-(CHCH2)-, wherein, p is equal to or more than 0 and equal to or less than 8, q is equal to or more than 0 and equal to or less than 8, and Ar<1> and Ar<2> correspond to aryl, aralkyl or aralkenyl, and n is equal to or more than 1 and equal to or less than 8, m is equal to or more than 1 and equal to or less than 8, Y is the same or different and represents alkoxyl or oxhydryl or O1/2; A is inorganic or organic acidic residue and actually exists as T-structure unit, and a is equal to or more than 0 and equal to or less than 2, b is equal to or more than 0 and equal to or less than 1, c is equal to or more than 0, c<*> is equal to or more than c, (a+b) is equal to or more than 0 and equal to or less than 3 and x is equal to or more than 2. The amino functional polysiloxane is also used as the binder between inorganic and organic surfaces or used in the process of coating organic polymer to inorganic surfaces, and the thickness of amino functional polysiloxane layer is less than 800nm.

The invention discloses an electroactive polymer with water solubility and biological degradability, which is prepared by a method comprising the following steps: preparing sodium polyaldehyde alginate by oxidizing sodium alginate with sodium periodate; preparing eigenstate phenyl/amino end-capped aniline oligomer by an oxidative coupling method; reducing the eigenstate phenyl/amino end-capped aniline oligomer to obtain fully reducedphenyl/amino end-capped aniline oligomer; and introducing the fully reducedphenyl/amino end-capped aniline oligomer into the sodium polyaldehyde alginate by the reaction of terminal amino in the fully reducedphenyl/amino end-capped aniline oligomer and the aldehyde in the sodium polyaldehyde alginate to obtain the aniline oligomer modified sodium polyaldehyde alginate. The invention also discloses a preparation method and application of the polymer. The polymer has the advantages of biocompatibility, water solubility, electroactive, degradability and the like; the preparation method of the electroactive polymer is simple in process and easy to control; and the electroactive polymer can be used in the field of injectable tissue engineering bracket materials or manufacturing of biological medicinal devices requiring electroactive.

The preparation method and application of the water-based polyurea modified epoxy emulsion curing agent of the present invention. In the water-based polyurea modified epoxy resin curing agent, a compound containing a non-ionic hydrophilic segment is introduced into the segment, which improves the brittleness of the cured product film, enhances the compatibility with the epoxy emulsion, and improves the Toughness of the epoxy emulsion, while making the curing agent water-soluble. The polyurea segment is introduced into the epoxy resin to make the cured paint film have superior water resistance, solvent resistance, flexibility, and higher strength, thus possessing the excellent characteristics of polyurea and overcoming the epoxy resin itself. Shortcomings. The curing agent synthesized by this method solves the problems of the first-generation and second-generation curing agents, removes small-molecule active agents and small-molecule polyamines, and improves the compatibility between the curing agent and the emulsion, thereby improving the coating film. Excellent mechanical properties and water resistance.