169 results about "Gardenia Fruit" patented technology

The invention relates to a method for aqueous enzymatic extraction of gardenia oil. The method adopts gardenia fruits as raw materials, which are subjected to crushing, enzymolysis and centrifugation, thus obtaining the gardenia oil. The gardenia oil prepared by the invention has high yield and high quality, is easy to refine, and maintains the natural nutrients and function of gardenia oil. Compared with the traditional squeezing method and organic solvent extraction method, the method has the advantages of simple production equipment, safe operation, less pollution, and low energy consumption, etc.

The present invention relates to a Chinese medicine lotion for treating jaundice in newborn. Said lotion can make the medicine be directly fed into blood by means of skin absorption, can promote blood circulation and raise spleen and stomach function, and can promote normal bile excretion so as to quickly eliminate jaundice in newborn. Said lotion is made up by using 15 Chinese medicinal materials of capillaris, rhubarb, gardenia fruit, bupleurum root, curcuma tuber, moneywort, plantago seed and others through a certain preparation method.

The invention discloses a method for preparing crocetin and crocin, which comprises the following steps: preparing a gardenia fruit extracting solution with ethanol under the conditions of ultrasonic waves, and concentrating the extracting solution to obtain an extract; and dissolving the extract in a polyethylene glycol aqueous solution, and selectively extracting with solvent to obtain crocetin and crocin. The invention does not need the chromatographic column separation process, has the advantages of simple operational method, and high product yield and purity, and is suitable for industrial production.

The invention provides a method for dyeing cotton fiber fabric through natural plant dye .According to the method, the natural plant dye prepared from gardenia fruit is adopted for dyeing the cotton fiber fabric into blue, the gardenia fruit is subjected to the steps of crushing, screening, plant oil and pectin removing, purification, concentration, macroporous resin column applying, cellulase adding and the like, and then the natural plant dye is obtained; the cotton fiber fabric is subjected to pretreatment so that surface impurities can be removed, then a setting machine is used for soaking the cotton fiber fabric twice and rolling the cotton fiber fabric twice, then sodium bicarbonate is used for treatment, rare earth or a rare earth derivative is added, then the obtained plant dye is added, the cotton fiber fabric is dyed into blue, and finally water washing, soaping, rinsing, dehydrating, drying and setting are carried out to obtain the blue cotton fiber fabric .According to the dyeing method, the natural plant dye prepared from the gardenia fruit is adopted for dyeing the cotton fiber fabric into blue, the dyeing effect is good, precise control over the whole process is easy, large-scale production can be carried out, and the cotton fiber fabric obtained through dyeing has a natural antibacterial effect.

The invention discloses a method for preparing high-purity gardenoside. The method comprises the following steps of: extracting and concentrating gardenia fruits serving as raw materials with water, and removing a great number of saccharide substances by an alcohol precipitation method; then extracting the raw materials with an appropriate single organic solvent; performing preliminary enrichment on gardenoside; finally absorbing and desorbing macroporous resin on gardenoside liquor after the preliminary enrichment to obtain gardenoside coarse crystals; and recrystallizing the gardenoside coarse crystals to obtain high-purity products. The method has the following advantages that: 1, the extraction method is fast and thorough; 2, the water extract is precipitated by ethanol to make the extraction operation have no emulsification phenomena so as to greatly shorten extraction time; and 3, the single solvent for extracting is convenient to recycle in industrial production so as to greatly reduce the production cost.

The present invention provides an ointment for external application for curing various burns, scalds, wound ulcera, nonunion of wound and osteomyelitis with the obvious therapeutic effect, and its preparation process includes the following steps: placing 25 Chinese medicinal materials of lonicera flower, rhubarb, coptis root, phellodendron bark, gardenia fruit, Chinese ilex leaf, dried / fresh rehmannia and others as raw material in sesame oil with 360-400 deg.C, deep-frying until scorched, removing residue, adding beesmax to obtain paste-like material, cooling to 60 deg.C, addinkg cutch powder, borneol powder and musk powder, stirring them, high-temp. steam sterilizing and botting so as to obtain the invented ointment which is low in cost, can eliminate wound infection, can promote tissue regeneration, and can make healed wound have no obvious and clear scar.

The present invention relates to a Chinese medicine for curing keratitis. Its raw material composition includes: coptis root, puccoon, gardenia fruit, buddleia flower, eriocaulon scape and flower and large gentian root, every 15g and ash bark 8g; it also includes several auxiliary prescriptions: for external contraction fever adding schizonepeta, forsythia fruit and lonicera flower, every 10g; for liver channel damp-heat adding gentian root and scutellaria root, every 12g; for exuberant heat toxin adding isatis root, isatis leaf and Yedo violet, every 20g; and for vacuity fire flaming upward adding phellodendron bark and chrysanthemum flower, every 12g.

The invention provides a production method of a gardenia yellow pigment, which comprises the following steps: a) extracting gardenia fruit powder to obtain a first pigment solution; b) purifying the first pigment solution with macroporous adsorption resin to obtain a second pigment solution; c) performing ultrafiltration of the second pigment solution by an ultrafiltration membrane to obtain a filtrate, wherein the ultrafiltration membrane is an ultrafiltration membrane with a molecular weight cutoff of 20000 dalton-100000 dalton; d) concentrating the filtrate obtained in step c) by a nanofiltration membrane to obtain the gardenia yellow pigment, wherein the nanofiltration membrane is a nanofiltration membrane with a molecular weight cutoff of 100 dalton-500 dalton. When the gardenia yellow pigment obtained by the production method provided by the invention is prepared into a preparation, precipitates are not easy to generated during refrigeration, and the preparation has a wide application scope. In addition, the production method of the gardenia yellow pigment of the invention has a simple process, and high production efficiency, and is applicable to industrial production.

The invention discloses a method of using gardenia to dye natural fibers. The method comprises the following steps that: gardenia fruit is pulverized, put into a pot to decoct a dyeing solution for 30 minutes and filtered, which is repeated for three times, and dyeing solutions are mixed for dye bath; a natural fiber dyed object after dyeability treatment is put into a dyeing vat for dyeing, and then is taken out from the dyeing vat and put into a mordanting vat for mordanting; the mordanting treatment is carried out at normal temperature; the dyed object after mordanting is taken out from the mordanting vat and put into the dyeing vat again for redyeing; after dyeing is finished, the dyed object is taken out from the dyeing vat, washed and dried, and then the dyeing process is completed. A gardenia dyeing technique can use one species of gardenia to dye a natural fiber into a plurality of colors, thereby utilizing one material efficiently. The gardenia dyeing technique is a full-ecologic dyeing technique, which has the advantages of saving energy, protecting environment, contributing to health, etc.

The invention discloses an ultrasonic extracting process for gardenia yellow pigment. The process comprises the steps of mixing gardenia fruit powder and an ethanol-water solution having a volume concentration of 71-73% with the ratio of the solution to the powder (V / m) being 23-24 mL : 1 g; extracting for 1.1-1.2 hours with ultrasonic at a temperature of 51-52 DEG C twice, wherein the ultrasonic frequency is 27 kHz-31 kHz; and mixing the obtained extracting solutions of the gardenia yellow pigment. The invention also discloses an optimized method of response surface methodology used in the extracting process for the gardenia yellow pigment. The optimized method sets four variables of the volume concentration of ethanol in the ethanol water solution, the liquor-to-material ratio of the gardenia fruit powder and the ethanol water solution, extracting temperature and extracting time, and performs an optimization by using a design expert soft according to a Box-Behnken design principle. By adopting the extracting process for the gardenia yellow pigment, an extraction rate of the gardenia yellow pigment is improved.

The present invention discloses a fingerprint chromatogram determination method of Chinese medicine injection preparation made up by using (by weight portion) 1000-1400 portions of sweet wormwood, 600-900 portions of lonicera flower and 500-700 portions of gardenia fruit. Said determination method adopts liquid-phase chromatography and gas-phase chromatography to make determination so as to raise the quality control of Reduning injection.

The present invention relates to a Chinese medicine liniment for external application for curing scald and burn. Said Chinese medicine has obvious effects for relieving inflammation, stopping pain and subduing swelling, and is made up by using gardenia fruit, coptis root, phellodendron bark and rhubarb as main medicinal materials, boiling them in sesame oil to make juice, then adding musk so as to oblain the invented liniment.

The invention discloses a Chinese medicinal preparation for treating viral myocarditis, which is prepared from the following raw materials in part by weight: 30 to 60 parts of ligularia japonica, 25 to 50 parts of many-headed savory, 20 to 40 parts of honeysuckle flower, 20 to 40 parts of isatis indigotica fort, 15 to 30 parts of scutellaria laterifolia, 15 to 30 parts of cortex moutan, 12 to 24 parts of gardenia fruit, 20 to 40 parts of danshen root, 10 to 20 parts of bamboo leaf and 6 to 18 parts of mix-fried liquoric root. The Chinese medicinal preparation for preventing and curing the viral myocarditis has the effects of soothing sinews and quickening network vessels, dissipating stasis and relieving noxious gas, diminishing inflammation, relieving pain, improving disease resistance of bodies, dilating blood vessels and improving arterial blood circulation, and has exact curative effect of preventing and curing the viral myocarditis. The Chinese medicinal preparation has the effective rate of 100 percent and the cure rate of 94 percent when taken in 60 days for the general viral myocarditis.

The present invention discloses a preparing method of gardenia yellow pigment, which comprises the following steps: powder of gardenia fruit after being crashed is extracted in ethanol water in a super-sound reverse current way; filter liquid and filter residue are obtained by filtering after being extracted; the filter liquid is processed in a micro-filtration way, and then, is purified by macroporous resin to obtain gardenia yellow pigment solution; the ethanol content in the ethanol water is 40 % to 60%; a ratio of the powder to the ethanol water is 1kg to (5-7) L; and the temperature of the ethanol water is 47 to 53 DEG C. The titer of the gardenia yellow pigment obtained by the preparing method of gardenia yellow pigment is high.

The invention discloses a method for preparing high-purity geniposide. The method comprises the following steps of: extracting active ingredients from gardenia fruits by using a 75 mass percent ethanol aqueous solution or water under the ultrasonic wave condition; extracting extractum obtained after concentration by using ethyl acetate; adding polymers such as sodium carboxymethylcellulose, polyacrylamide, polyethylene glycol and the like into a retained bottom phase aqueous solution and dissolving completely; extracting by using a mixed solvent of normal butanol and ethyl acetate; merging an upper phase organic solution; decoloring by using active carbon; concentrating under reduced pressure and performing vacuum drying to obtain a geniposide crude product; and recrystallizing the geniposide crude product to obtain the high-purity geniposide. The method is easy to operate; the production cycle is short; yield and purity of the products are high; and the method is suitable for industrialized mass production.

The invention discloses a medicament for improving eyesight. In the medicament, szechuan tangshen root, astragalus, large-headed atractylodes, Chinese angelica, rehmanniae vaporata, red paneoy root, rehmanniae praeparatum, gardenia fruit, medlar, eucommia bark, south dodder seed, raspberry, root of red-rooted salvia, notoginseng root, pale butterflybush flower, blackend swallowwort root, fish poison yarn and chrysanthemum are ground into 200-mesh powder, and are mixed uniformly, sterilized and packaged, wherein each bag contains 5 grams of medicament. The medicament is mainly used for treating patients who suffer from blurred vision caused by symptoms such as deficiency in kidney and yang, deficiency in blood and qi, diabetes mellitus, retinopathy, fundus hemorrhage, vitreous opacity, glaucoma or optic nerve pathological changes and the like, and 50 patients who suffer from the blurred vision are selected in the outpatient service of a hospital randomly to take the medicament. In the administration method and dosage, adults take twice every day, and takes 5 grams every time; for the children, the dosage is reduced by half; and 20 days is one treatment course, the total cure rate is 69 percent, the total cure rate of two treatment courses is 86.3, and the cure rate of three treatment course is 97.2 percent.

The invention discloses a traditional Chinese medicine composition for treating diabetes. The traditional Chinese medicine composition is prepared from the following medicinal materials: astragalus membranaceus, codonopsis, Indian buead, Chinese yam, black beans, ginseng, soroseris umbrellata, caudate sweetleaf flower, dwarf lilyturf tuber, mongolian snakegourd root, root of rehmannia, pulp of dogwood fruit, polygonatum sibiricum, Chinese magnoliavine fruit, yam rhizome, figwort root, prepared rhizome of rehmannia, palmleaf raspberry fruit, persimmon exocarp, coptis chinensis, lalang grass rhizome, Japanese honeysuckle stem, actinidia arguta, honeysuckle flower, weeping forsythiae capsule, heartleaf houttuynia herb, sharpleaf galangal fruit, gypsum, dendrobium, conic gymnadenia tuber, trillium tschonoskii maxim, gardenia fruit, white mulberry root-bark, barbary wolfberry fruit, rhizoma alismatis, stevia rebaudiana, fragrant solomonseal rhizome, flatstem milkvetch seed, corn silk, scorched hawthorn fruit, rhizoma atractylodis, largehead atractylodes rhizome, pinellia tuber, dried orange peel, officinal magnolia bark, silkworm chrysalis, hyacinth bean, round cardamom fruit, fructus amomi, pseudo-ginseng flower, earthworm, Chinese angelica, red paeony root, szechuan lovage rhizome, safflower, peach seed, rhubarb, cassia twig, compound of glauber-salt and liquorice and giant knotweed rhizome. Proved by clinical trials, the traditional Chinese medicine composition disclosed by the invention can be used for safely and effectively treating diabetes.

The invention provides a method for simultaneously preparing six iridoid glycoside components from jasmine flowers efficiently and rapidly. The method comprises the steps that jasmine fruit alcohol extracts are subjected to macroporous resin coarse separation, reverse phase intermediate-pressure preparation solution liquid chromatogram enriched flow separation and reverse phase high-pressure separation and purification, and the six monomer compounds with the purity higher than 95% or above can be obtained. The method can enlarge the laboratory separation scale and improve the purifying efficiency; the preparation technology is simple, the cost is low, the extraction efficiency is high, more importantly, samples are not wasted, and the crystallization purity is high.

The invention relates to a plaster for treating heumatism. The plaster is characterized by being prepared from the following raw medicinal materials by weight: 15g of radix aconiti, 15g of radix aconiti kusnezoffii, 15g of ephedra herb, 10g of herba asari, 15g of rhizoma pinelliae, 15g of cortex eucommiae, 15g of semen strychni, 10g of peach kernels, 10g of flos carthami, 15g of black-striped snake, 15g of scorpion, 15g of scolopendra, 15g of stiff silkworm, 20g of drynaria rhizome, 15g of salivia chinensis, 20g of radix angelicae sinensis, 15g of olibanum, 15g of myrrh, 15g of cassia twig, 20g of ground beetle, 20g of lumbricus, 20g of leech, 15g of pericarpium citri reticulatae viride, 15g of fructus chaenomelis, 15g of notopterygium root, 15g of radix angelicae pubescentis, 15g of Ligusticum wallichii, 15g of radix angelicae dahuricae, 15g of dipsacus roots, 15g of rape gardenia fruit, 20g of radix notoginseng, and 15g of raw arisaema.

The invention discloses a process technology of extracting a crocin-type component from gardenia. The process technology includes following steps: (1) crushing gardenia fruit into crude powder and placing the crude powder in an ultrasonic cleaning trough; (2) adding 75% ethanol by 8 times to the crude powder and performing ultrasonic alcohol extraction at a certain temperature for 1 h to obtain an extract; (3) filtering-out the extract, adding 75% ethanol by 6 times and performing ultrasonic alcohol extraction at a certain temperature for 1 h to obtain an extract to obtain an extract; (4) filtering-out the extract, mixing the two extracts and performing reduced-pressure concentration to the mixed extract in a rotary evaporator to a relative density of 1.15-1.20 to obtain a concentration liquid; (5) adding 80% ethanol by 4 times and refrigerating the concentration liquid for 10 h, filtering the concentration liquid to remove precipitation and performing reduced-pressure concentration to a supernate to the relative density of 1.15-1.20; (6) adding 80% ethanol by 8 times and refrigerating the concentration liquid for 10 h to obtain a precipitation; (7) dissolving the precipitation in a proper amount of water to obtain a water solution and feeding the water solution into macroporous resin columns comprising types of D101 and AB-8 in series, washing the water solution until the water solution is almost colorless with 15% ethanol and eluting the water solution with 85% ethanol; and (8) collecting an eluted liquid and reduced-pressure drying the eluted liquid to obtain the crocin-type component.

The invention contemplates a method for sterilizing protein or collagen-based hard and soft tissues, from animal and human donors or created synthetically by exposure to genipin, an active compound found in gardenia fruit extract. Genipin sterilizes the tissues through crosslinking the organic framework of microbes while maintaining or enhancing mechanical strength of the tissue graft by stabilizing the collagen backbone with crosslinks bone allografts experience significant and repetitive loads during their duty cycle, sterilizing bone allografts without causing a loss in biomechanical properties is quite important.

The present invention discloses an effective component extracted from gardenia fruit, it contains (by wt%) at least 50% of gardenoside. Said invention also discloses preparation method of said effective component, medicine composition containing said effective component and application of said effective component in preparation of medicine for preventing and / or curing senile dementia.

The present invention discloses a quality control method of Chinese medicine composition for curing infantile common cold. Said method adopts thin-layer chromatography to identify active effective components of scutellaria root, arctium seed, gardenia fruit and forsythia fruit, and utilizes high-performance liquid determination method to determine the content of baicalin.

The present invention relates to a plant moisture-retaining functional liquor. It is made up by using (by wt%) 11-13% of chaenomeles fruit, 12-14% of Chinese yam, 11-13% of chrysanthemum flower, 3-5% of sandalwood, 5-7% of lotus embryo, 6-8% of astragalus root, 7-9% of sophora flower, 6-8% of gardenia fruit, 3-5% of Chinese angelica root, 5-7% of scutellaria root, 7-9% of pueraria root and 12-14% of cuscuta seed through a certain preparation process.

The invention relates to a process for extracting gardenia yellow from gardenia. The process comprises the following steps of: crushing raw materials, performing water diacolation for extracting, performing micro-filtration, performing macroporous resin column chromatography, separating and purifying, concentrating and drying products and activating and regenerating columns, wherein in the step of performing water diacolation for extracting, dry gardenia fruits are crushed into large granules, and the large granules are soaked in pure water and are subjected to the diacolation at normal temperature to be extracted; in the step of performing micro-filtration, a water extracting solution is subjected to the micro-filtration by using 0.2 to 1 micrometer of ceramic membrane to obtain a completely-clarified filtrate; in the method for performing loading adsorption continuously, three sections of columns are connected in series to perform the loading adsorption, and the third section of column is separated and purified further; and in the step of activating and regenerating columns, the efficient macroporous resin columns are separated continuously under high pressure and are activated and regenerated on line. According to the process, a constant pressure technology is upgraded to a pressurization technology, so that the adsorptive capacity and separation efficiency of the resin columns are improved; and according to the high-end gardenia yellow products, the color scale of the prepared gardenia yellow is over 500, an optical density (OD) value is below 0.2, and the content of geniposide is less than 1 percent by high performance liquid chromatography (HPLC) detection on the basis of the color scale of 500.

The invention relates to a method for planting gardenia jasminoides, relates to the field of cultivation of Chinese herbal medicines. The method comprises the following steps: (1), selecting cutting slips; (2), processing the cutting slips; (3), performing cuttage; (4), transplanting; (5), performing field management; (6), timely harvesting. According to the method for planting gardenia jasminoides, provided by the invention, the survival rate of cuttings is effectively improved, rooting is accelerated, the growth cycle is shortened, the planting time is shortened, the cost is reduced, the cultivated gardenia jasminoides has completely filled fruits, high yield and stable quality; besides, the planting method is simple, easy to operate, suitable for large-scale cultivation and has good economic benefits.

The invention provides a production method for gardenia yellow pigment. The production method comprises the following steps of: (a) lixiviating gardenia fruit powder to obtain first pigment solution; (b) purifying the first pigment solution with macroporous adsorption resin to obtain second pigment solution; and (c) refining the second pigment solution with ion exchange resin to obtain gardenia yellow pigment, wherein the ion exchange resin contains a sulfonic group, acylamino group or amino group. The gardenia yellow pigment obtained by the production method provided by the invention has the advantages of less impurities, high color number and low gardenoside content; an aqueous solution of the gardenia yellow pigment has high clarity and low probability of producing precipitate under acidic environment; and the gardenia yellow pigment has broader application range.

The invention provides external-use paste which can thoroughly cure chronic rhinitis, chronic sinusitis and allergic rhinitis. The traditional Chinese medicine ointment comprises main materials and auxiliary materials, wherein the main materials comprise, in parts by weight, 30-60 parts of magnolia flowers, 30-60 parts of siberian cocklour fruit, 40-70 parts of dahurian angelica root, 20-60 parts of mint, 30-60 parts of cicada slough, 30-60 parts of blister beetle, 20-40 parts of manchurian wildginger and 30-60 parts of gardenia fruit; the auxiliary materials comprise in parts by weight, 100-300 parts of honey and 50-150 parts of rice wine. The rhinitis paste has the characteristics as follows: 1, the rhinitis paste is an ancestral secret prescription, has a reliable curative effect and can cure chronic rhinitis, chronic sinusitis and allergic rhinitis; 2, the rhinitis paste is simple and convenient to use, is only pasted on acupoints and has few side effects; 3, the effect is good, and relapse is prevented after healing; 4, the rhinitis paste takes effect rapidly and can relieve the symptoms after being pasted for 2 hours; 5, the rhinitis can be thoroughly cured after a patient uses the paste 1-3 times according to the time of the illness condition and the illness degree.

The present invention discloses a Chinese patent medicine with the functions of removing fire from the liver, nourishing yin and suppressing hyperactive yang and resolving the hard lumps for curing hyperthyreosis and related diseases with obvious therapeutic effect. Said Chinese patent medicine is made up by using 16 Chinese medicinal materials of prunella spike, white peony root, shancigu bulb, kelp, mulberry leaf, gardenia fruit and others.