PET polyester film antistatic agent and preparation method thereof
A technology of antistatic agent and polyester film, applied in the field of antistatic agent and its preparation, can solve problems such as limited application, and achieve the effect of reducing surface resistance and high transparency
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[0032] Example 1
[0033] Synthesis of aliphatic polyester oligomers. Take 146g adipic acid, 62g ethylene glycol, and 1% mass fraction of p-toluenesulfonic acid, mix and esterify at 160°C for 1h. Then vacuumize the system to reduce the vacuum degree of the system to below 100 Pa, and continue to polycondensate for 0.5 h. The product was then cooled, and THF was added to dissolve the product. Precipitating in ether and drying to obtain an aliphatic polyester oligomer with a molecular weight of 400 g / mol.
[0034] Synthesis of unsaturated aliphatic polyester oligomers. Take 60 g of the above aliphatic polyester oligomer and 14 g of maleic anhydride, and the molar ratio of the two is 1:1. After mixing, esterify at 160°C for 4h. After cooling, THF was added to dissolve the product, followed by precipitation in ether, and then drying to obtain unsaturated aliphatic polyester oligomer. The molecular weight is 500g / mol.
[0035] Synthesis of unsaturated aliphatic polyester oligomer a...
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[0036] Example 2
[0037] Synthesis of aliphatic polyester oligomers. Take 146g adipic acid, 62g ethylene glycol, and 1% mass fraction of p-toluenesulfonic acid, mix and esterify at 160°C for 1h. Then vacuumize the system to reduce the vacuum degree of the system to below 100 Pa, and continue to polycondensate for 0.5 h. The product was then cooled, and THF was added to dissolve the product. Precipitating in ether and drying to obtain an aliphatic polyester oligomer with a molecular weight of 400 g / mol.
[0038] Synthesis of unsaturated aliphatic polyester oligomers. Take 60 g of the above aliphatic polyester oligomer and 14 g of maleic anhydride, and the molar ratio of the two is 1:1. After mixing, esterify at 160°C for 4h. After cooling, THF was added to dissolve the product, followed by precipitation in ether, and then drying to obtain unsaturated aliphatic polyester oligomer. The molecular weight is 500g / mol.
[0039] Synthesis of unsaturated aliphatic polyester oligomer a...
Example Embodiment
[0040] Example 3
[0041] Synthesis of aliphatic polyester oligomers. Take 146g adipic acid, 62g ethylene glycol, and 1% mass fraction of p-toluenesulfonic acid, mix and esterify at 160°C for 1h. Then vacuumize the system to reduce the vacuum degree of the system to below 100 Pa, and continue to polycondensate for 0.5 h. The product was then cooled, and THF was added to dissolve the product. Precipitating in ether and drying to obtain an aliphatic polyester oligomer with a molecular weight of 400 g / mol.
[0042] Synthesis of unsaturated aliphatic polyester oligomers. Take 60 g of the above aliphatic polyester oligomer and 14 g of maleic anhydride, and the molar ratio of the two is 1:1. After mixing, esterify at 160°C for 4h. After cooling, THF was added to dissolve the product, followed by precipitation in ether, and then drying to obtain unsaturated aliphatic polyester oligomer. The molecular weight is 500g / mol.
[0043] Synthesis of unsaturated aliphatic polyester oligomer a...
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