Test paper for detecting trace elements and production method thereof
A technology for detecting test strips and trace elements, applied in biological testing, measuring devices, material inspection products, etc., to achieve the effects of easy use, low cost for one-time use, and fast and accurate test results
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[0030] The present invention also provides a preparation method of calcium element detection test paper, comprising the steps of:
[0031] (1) Preparation of impregnation solution: 3.5g-4.5g buffer solution, 50g-100g surfactant, 2.5g-5.5g concealing agent, 0.1g-0.9g calcium indicator, 0.9g-1.5g ethylenediaminetetra Acetic acid was added to the volumetric flask, and the volume was adjusted to 1000ml;
[0032] Wherein, the buffer solution is prepared with sodium hydroxide, the surfactant is a combination of polyvinylpyrrolidone and polyethylene glycol, and the masking agent is a combination of sodium tartrate and 8-hydroxyquinoline;
[0033] (2) Soak the porous nanomaterial in the dipping solution, take it out after soaking for 20 minutes, and put it in an oven for drying, the temperature of the oven is 30-50°C.
[0034] Preferably, in the preparation method of the calcium element detection test paper of the present invention, the pH value of the soaking solution in step (1) is...
Embodiment 1
[0036] This example provides a method for preparing a test paper for detecting calcium deficiency in children's urine, comprising the following steps:
[0037] (1) Preparation of impregnation solution: 3g sodium hydroxide, 25g polyvinylpyrrolidone, 30g polyethylene glycol, 5.5g tartaric acid, 0.05g calcium indicator, 0.9g EDTA are added in the volumetric flask, and the volume is adjusted to 1000ml with distilled water;
[0038] (2) Making porous nanomaterials: Soak 1g of activated carbon with a specific surface area of 1200m2 / g and an average pore diameter of 2.5nm in concentrated nitric acid with a mass fraction of 70% and stir at 65°C for 2 hours, filter, wash with water, and dry for later use . Take 1g of acrylamide, add 50ml of distilled water, and heat at 45°C until completely dissolved. Then add 50ml of methanol and a small amount of ammonium persulfate in turn, stir evenly, pour into a container with activated carbon and stir for 10 hours at low temperature. Then, t...
Embodiment 2
[0042] This embodiment provides a method for preparing a test paper for detecting excess calcium in children's urine, comprising the following steps:
[0043] (1) Preparation of impregnation solution: 3g sodium hydroxide, 25g polyvinylpyrrolidone, 30g polyethylene glycol, 3g tartaric acid, 1.5g calcium indicator, 1.5gEDTA are added in the volumetric flask, and the volume is adjusted to 1000ml with distilled water;
[0044] (2) Making porous nanomaterials: soak 1g of activated carbon with a specific surface area of 1200m2 / g and an average pore diameter of 5nm in concentrated nitric acid with a mass fraction of 70% at 65°C for 2 hours, filter, wash and then dry for later use. Take 1g of acrylamide, add 50ml of distilled water, and heat at 45°C until completely dissolved. Then add 50ml of methanol and a small amount of ammonium persulfate in turn, stir evenly, pour into a container with activated carbon and stir for 10h at low temperature. Then, the container was reacted at a ...
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