A kind of water-soluble lubricant for papermaking and preparation method thereof
A lubricant and water-soluble technology, which is applied in the field of paper-making water-soluble lubricants and its preparation, can solve problems such as complex processes, and achieve the effect of improving smoothness and gloss, improving smoothness and gloss
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Embodiment 1
[0036] Synthesis of embodiment 1 water-soluble lubricant:
[0037] Step 1, add 100g of stearic acid, 10g of sodium phosphate, 5g of diethanolamine and 135g of deionized water into the reaction kettle, mix well, dissolve completely, and heat up to 90°C;
[0038] Step 2, at 90°C, add 20g of isomeric alcohol polyoxyethylene ether dropwise for 1 hour; after the dropwise addition, keep warm at 90°C for 1 hour;
[0039] Step 3: Cool down the heat-preserved mixed solution to 20° C., add 0.01 g of bronopol, continue stirring for 10 minutes, and filter the mixture through a 100-mesh sieve.
[0040] In step 4, the obtained water-soluble lubricant has a weight solid content of 49.7wt%, a viscosity of 634 mPa.s (measured by NDJ-1 rotational viscometer), and pH=7.18 (measured by PHS-3C precision pH meter).
Embodiment 2
[0041] The synthesis of embodiment 2 water-soluble lubricants:
[0042] Step 1, add 100g of palmitic acid, 30g of potassium phosphate, 20g of sodium hydroxide and 1800g of deionized water into the reaction kettle, mix well, dissolve completely, and heat up to 70°C;
[0043] Step 2: Add 50 g of isomeric alcohol polyoxyethylene ether mixture dropwise at 70°C for 3 hours; after the dropwise addition, keep warm at 70°C for 3 hours;
[0044] Step 3, cool down to 40°C, add 0.05g bronopol, 0.1g 5-chloro-2-methyl-4-isothiazolin-3-one, 0.05g 2-methyl-4-isothiazoline-3- Ketone, continued to stir for 10 minutes, and filtered the discharge with a 100-mesh sieve.
[0045] Step 4, the obtained water-soluble lubricant has a weight solid content of 10.9wt%, a viscosity of 11 mPa.s (measured by NDJ-1 rotational viscometer), and pH=10.81 (measured by PHS-3C precision pH meter).
Embodiment 3
[0046] The synthesis of embodiment 3 water-soluble lubricants:
[0047] Step 1, add 50g of palmitic acid, 50g of oleic acid, 10g of potassium phosphate, 10g of sodium phosphate, 5g of potassium hydroxide, 5g of triethylenediamine and 680g of deionized water into the reactor, mix well, dissolve completely, and heat up to 80 ℃;
[0048] Step 2, at 80°C, add 40g of isomeric alcohol polyoxyethylene ether dropwise for 2 hours; after the dropwise addition, keep warm at 80°C for 2 hours;
[0049] Step 3, cool down to 25°C, add 0.07g 5-chloro-2-methyl-4-isothiazolin-3-one, 0.05g 2-methyl-4-isothiazolin-3-one, and continue stirring for 10 minutes , and filter the discharge with a 100-mesh sieve.
[0050] Step 4, the weight solid content of the obtained water-soluble lubricant is 20.16wt%, the viscosity is 48mPa.s (measured by NDJ-1 rotational viscometer), and pH=8.69 (measured by PHS-3C precision pH meter).
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