ZnGaNO-polymer self-cleaning hybrid membrane and preparation method thereof
A polymer membrane, polymer technology, applied in chemical instruments and methods, membrane, membrane technology, etc., can solve problems such as inconvenience and increase operating costs, and achieve the effects of simple operation, low production cost, and good hydrophilicity
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Embodiment 1
[0032] Disperse 0.005g and 0.01g of ZnGaNO particles in 1.8mL of N-methylpyrrolidone (NMP), and dissolve 1g of polysulfone in 4mL of NMP; then add the ZnGaNO dispersion into the polysulfone solution, stir, and perform ultrasonic treatment , to obtain a uniform casting solution; after the prepared casting solution was left to stand for degassing, it was directly coated on a clean glass plate with a glass rod; the glass plate was placed horizontally and immersed in a water bath at 30°C, and the prepared film was used Rinse with plenty of water to remove residual solvent in the membrane, and store in water.
[0033] Under the operating pressure of 0.2MPa, the pure water flux of the obtained ZnGaNO particle content of 0.5% and 1% ZnGaNO-polysulfone hybrid ultrafiltration membrane is 254L / m respectively. 2 h, 356L / m 2 h (the pure water flux of the pure polysulfone ultrafiltration membrane prepared under the same parameters is only 189L / m 2 h), the retention rate of the bovine ser...
Embodiment 2
[0035] Disperse 0.01g ZnGaNO particles in 1.8mL N-methylpyrrolidone (NMP), dissolve 1g polysulfone in 4mL NMP; then add the ZnGaNO dispersion into the polysulfone solution, stir, and perform ultrasonic treatment to obtain a uniform cast film liquid; after the prepared film casting solution is left to stand for defoaming, it is directly coated on a clean glass plate with a glass rod; the glass plate is placed horizontally and immersed in a water bath at 30°C, and the prepared film is washed with a large amount of water to remove Solvent remaining in the film and kept in water.
[0036] Under the operating pressure of 0.2MPa, the measured pure water flux of the ZnGaNO-polysulfone hybrid ultrafiltration membrane is 356L / m 2 h. After the membrane is polluted by methylene blue, the pure water flux drops to 84L / m 2 h, After irradiating with a visible light source for 30 minutes, the methylene blue adsorbed on the surface of the membrane is basically degraded, the blue color disapp...
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