Method for synthesizing P zeolite molecular sieve from rice husk
A technology of zeolite molecular sieve and rice husk, which is applied in the direction of crystalline aluminosilicate zeolite, etc., to achieve the effects of high whiteness, easy availability of materials, and reduced production costs
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Embodiment 1
[0031] A kind of method that embodiment 1 provides is that raw material synthetic P-type zeolite molecular sieve with rice husk, comprises the steps:
[0032] Rinse the rice husk, dry after removing impurities, and cook the rice husk with 10% sulfuric acid solution (the weight ratio of rice husk and 10% sulfuric acid solution is 1:2) for 1 hour; wash the rice husk after co-cooking with distilled water for 3 After drying, put it in a muffle furnace and keep it warm at 400°C for 5 hours to obtain rice husk ash; mix rice husk ash, sodium hydroxide and water, place it in a high-pressure reactor and seal it, heat it to 180°C and activate it at 0.5MPa Treat for 4 hours, add sodium aluminate and water, adjust the molar ratio of each material in the lye to: Al 2 o 3 : SiO 2 : Na 2 O: H 2 O=1:2.6:3.5:85, add P-type zeolite seeds, stand and age at 60°C for 6 hours, then raise the temperature to 90°C, stir and crystallize for 6 hours, filter, wash, and then dry at 100°C After 2 hour...
Embodiment 2
[0034] A kind of method that embodiment 2 provides is that raw material synthetic P-type zeolite molecular sieve with rice husk, comprises the steps:
[0035] Rinse the rice husk, dry after removing impurities, and cook the rice husk with 15% sulfuric acid solution (the weight ratio of rice husk and 15% sulfuric acid solution is 1:2) for 2 hours; wash the rice husk after co-cooking with distilled water for 5 After drying, put it in a muffle furnace and keep it warm at 800°C for 1 hour to obtain rice husk ash; mix rice husk ash, sodium hydroxide and water, place it in a high-pressure reactor and seal it, heat it to 230°C and activate it at 0.5MPa Treat for 4 hours, add aluminum sulfate and water, adjust the molar ratio of each material in the lye to: Al 2 o 3 : SiO 2 : Na 2 O: H 2 O=1:3.3:4.5:180, add P-type zeolite seeds, stand and age at 80°C for 2 hours, then raise the temperature to 100°C, stir and crystallize for 3 hours, filter, wash, and then dry at 100°C After 2 ho...
Embodiment 3
[0037] A kind of method for the synthetic P-type zeolite molecular sieve of raw material with rice husk that embodiment 3 provides, comprises the steps:
[0038] Rinse the rice husks, dry them after removing impurities, and co-cook the rice husks with 12% sulfuric acid solution (the weight ratio of rice husks to 12% sulfuric acid solution is 1:2) for 1.5 hours; wash the rice husks after co-cooking with distilled water 4 times, after drying, put it in a muffle furnace and keep it warm at 650°C for 4 hours to obtain rice husk ash; mix rice husk ash, sodium hydroxide and water, put it in a high-pressure reactor and seal it, heat it to 210°C at 1.2MPa Activation treatment for 4 hours, adding aluminum nitrate and water, adjusting the molar ratio of each material in the lye to: Al 2 o 3 : SiO 2 : Na 2 O: H 2 O=1:2.8:4.1:120, add P-type zeolite seeds, stand and age at 80°C for 8 hours, then raise the temperature to 95°C, stir and crystallize for 4 hours, filter, wash, and then dr...
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