Preparation method of lotus leaf carbon nano material/regenerated cellulose blended fibers

A technology of regenerated cellulose and nanomaterials, applied in the field of blended regenerated cellulose preparation, to achieve the effects of low cost, good adsorption and deodorization effects, and abundant sources

Active Publication Date: 2017-02-08
QINGDAO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the prior art, there is no method for combining lotus leaves with regenerated cellulose to produce a blended fiber with better performance

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] The invention provides a method for preparing regenerated cellulose blended fibers of lotus leaf carbon nanomaterials, comprising the following preparation steps:

[0029] (1) Prepare high-performance lotus leaf carbon nanomaterials with lotus leaves as raw materials: pick and remove lotus leaves after collection, wash, freeze-dry, and then pulverize and sieve to obtain 100-mesh lotus leaf powder; take the lotus leaf powder in Calcined to black in a nitrogen atmosphere at 200°C for 60 minutes to obtain a pre-carbonized product; add potassium permanganate to the pre-carbonized product according to a weight ratio of 1:1, at a temperature of 50°C and a stirring speed of Stirring under the condition of 50r / min for 4h to obtain a precursor; drying the precursor at 50°C for 6h to obtain an intermediate product; subjecting the intermediate product to heat treatment to obtain product I, the conditions of the heat treatment are, at 10 Heat up to 600°C at a heating rate of °C / min...

Embodiment 2

[0033] Different from Example 1, a method for preparing regenerated cellulose blended fibers of lotus leaf carbon nanomaterials comprises the following preparation steps:

[0034] (1) Prepare high-performance lotus leaf carbon nanomaterials with lotus leaves as raw materials: pick and remove lotus leaves after collection, wash, freeze-dry, and then pulverize and sieve to obtain 50 mesh lotus leaf powders; take the lotus leaf powders in Calcined to black under argon atmosphere at 800°C for 60 minutes to obtain a pre-carbonized product; add phosphorus pentoxide to the pre-carbonized product according to the weight ratio of 1:5, at a temperature of 50°C and a stirring speed of Stirring at 300r / min for 10h to obtain a precursor; drying the precursor at 100°C for 12h to obtain an intermediate product; subjecting the intermediate product to heat treatment to obtain product I, the heat treatment conditions being, Raise the temperature to 1400°C at a heating rate of 20°C / min, and then...

Embodiment 3

[0038] Different from Example 1, a method for preparing regenerated cellulose blended fibers of lotus leaf carbon nanomaterials comprises the following preparation steps:

[0039] (1) Prepare high-performance lotus leaf carbon nanomaterials with lotus leaves as raw materials: pick and remove lotus leaves after collection, wash, freeze-dry, and then pulverize and sieve to obtain 70 mesh lotus leaf powder; take the lotus leaf powder in Calcined to black under argon atmosphere at 650°C for 30 minutes to obtain a pre-carbonized product; add phosphorus pentoxide to the pre-carbonized product according to the weight ratio of 1:3, at a temperature of 30°C and a stirring speed of Stirring at 250r / min for 8h to obtain a precursor; drying the precursor at 85°C for 10h to obtain an intermediate product; subjecting the intermediate product to heat treatment to obtain product I, the conditions of the heat treatment are as follows: The temperature was raised to 1000°C at a heating rate of 1...

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Abstract

The invention discloses a preparation method of lotus leaf carbon nano material/regenerated cellulose blended fibers. The method is characterized by comprising the following steps: (1) preparing a high-performance lotus leaf carbon nano material from lotus leaves; (2) blending the lotus leaf carbon nano material with a regenerated cellulose spinning solution; and (3) spinning the blended spinning solution by a wet spinning device, and forming fibers by a coagulating bath, thereby preparing the lotus leaf carbon nano material/regenerated cellulose blended fibers. The preparation method has the advantages of abundant raw material sources, low cost, simple preparation technique and no pollution, and can implement mass production. The prepared lotus leaf carbon nano material/regenerated cellulose blended fibers have favorable antimicrobial, adsorption and deodorization effects, and has higher added value than the common regenerated cellulose.

Description

technical field [0001] The invention belongs to the technical field of preparation of blended regenerated cellulose, and in particular relates to a preparation method of regenerated cellulose blended fiber made of lotus leaf carbon nanometer material. Background technique [0002] Regenerated fibers are chemical fibers made from natural polymers by chemical methods, and have basically the same chemical composition as the original polymers. Due to the characteristics of softness, comfort, breathability and environmental protection of regenerated cellulose fiber, the clothes woven by it are favored by consumers all over the world. Due to the reduction of cultivated land and the depletion of oil resources, the output of natural fibers and synthetic fibers will be more and more restricted; while people pay attention to the environmental protection performance in the process of textile consumption, the value of regenerated cellulose fibers has been reconsidered. Know and discove...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/02D01F1/10
CPCD01F1/10D01F1/103D01F2/02
Inventor 曲丽君田明伟杜敏芝迟淑丽赵洪涛赵壬海于荣荣
Owner QINGDAO UNIV
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