Method for improving reaction property of dissolving pulp board

A reactive and dissolving pulp technology, which is applied in textiles and papermaking, papermaking, and microbial/enzymatic cellulose treatment, etc. It can solve the problems of high energy consumption, high energy consumption, and water consumption, so as to avoid extra energy and solve high water consumption. , The effect of improving the reaction performance

Active Publication Date: 2017-02-08
FUJIAN AGRI & FORESTRY UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] At present, bio-enzyme treatment is often used at home and abroad to improve the reaction performance of dissolving pulp raw materials. The basic steps are: first disintegrate the dissolving pulp board to obtain dissolving pulp, and then add water to dilute the dissolving pulp to a low concentration state (low concentration state of dissolving pulp ), and in this low concentration state, cellulase is used to treat dissolving pulp fibers, and then the enzyme-treated pulp is concentrated; this treatment technology will cause a large amount of water consumption, and it will cost additional Extrude the water with the energy to squeeze out the water, which not only causes waste of water resources, but also consumes a lot of energy and high cost; in addition, in the state of low dissolving pulp concentration, the existence of a large amount of free water will affect the cellulase and dissolving pulp fiber binding effect, thereby reducing the efficiency of cellulase

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Embodiment 1 improves the reaction performance of eucalyptus wood prehydrolysis sulfate dissolving pulp board

[0030] First take the eucalyptus wood prehydrolyzed sulfate dissolving pulp board with a thickness of 0.25cm, and control its moisture content to 5%, and set aside; then take endo-cellulase to prepare a cellulase solution with a mass concentration of 5%, and use hydrogen phosphate Potassium adjusts the pH value of the cellulase liquid to 4.8 to obtain the cellulase liquid for use; then spray the cellulase liquid for use and water evenly on the dissolving pulp plate to be used successively, and the cellulase liquid for use The amount of spraying is 1mg / g dry pulp, and the water content of the dissolving pulp board after the spraying treatment is 40% (that is, the concentration of the dissolving pulp is 60%), and the reaction is prepared; then the dissolving pulp board is placed in a constant temperature and humidity chamber (temperature The temperature is 45°C ...

Embodiment 2

[0032] Embodiment 2 improves the reaction performance of hemlock acid sulfite dissolving pulp board

[0033] First take the hemlock acid sulfite dissolving pulp board with a thickness of 0.40cm, and control its moisture content to be 4%, and stand-by; then take endo-cellulase to prepare a cellulase solution with a mass concentration of 8%, and use Potassium hydrogen adjusts the pH value of the cellulase liquid to 5.5 to obtain the cellulase liquid for use; then spray the cellulase liquid for use and water evenly on the dissolving pulp plate to be used successively, and the cellulase for use The spraying amount of liquid is 0.01mg / g absolute dry pulp, and the water content of dissolving pulp board after spraying treatment is 30% (that is, the concentration of dissolving pulp is 70%), prepare reaction; Then dissolving pulp board is placed in constant temperature and humidity chamber (The temperature is 50° C., the humidity is 30%), and the reaction time is 2 weeks.

[0034] The...

Embodiment 3

[0035] Embodiment 3 improves the reaction performance of bamboo prehydrolysis sulfate dissolving pulp board

[0036] First take bamboo pre-hydrolyzed sulfate dissolving pulp board with a thickness of 0.10 cm, and control its moisture content to be 8%, and set aside; then take endo-cellulase to prepare a cellulase solution with a mass concentration of 10%, and use sodium hydrogen phosphate Adjust the pH value of the cellulase liquid to 5.0 to obtain the cellulase liquid for use; then spray the cellulase liquid for use and water evenly on the dissolving pulp plate to be used successively, and the cellulase liquid for use Spraying amount is 8mg / g absolute dry pulp, and the water content of dissolving pulp plate after spraying treatment is 20% (being that the concentration of dissolving pulp is 80%), prepare reaction; Then dissolving pulp plate is placed in constant temperature and humidity chamber (temperature is 50° C., humidity 20%), the reaction time is 5 hours.

[0037] The ...

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PUM

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Abstract

The invention provides a method for improving the reaction property of a dissolving pulp board. The method comprises the following steps of adopting the dissolving pulp board with the thickness being 0.05cm to 0.50cm, and controlling the moisture content of the dissolving pulp board to be 2 percent to 10 percent for standby use; adopting cellulase for preparing a cellulase solution with the mass concentration being 5 percent to 10 percent, adopting strong acidic-weak basic salt for adjusting a pH value of the cellulase solution to be 4.5 to 5.5, and obtaining a cellulase solution for standby use; sequentially and uniformly spraying the cellulase solution for standby use and water on the processed dissolving pulp board, and preparing to react; putting the dissolving pulp board into a constant temperature and humidity room for reacting, wherein the temperature of the constant temperature and humidity room ranges from 40 to 60 DEG C, and the humidity of the constant temperature and humidity room is consistent to the moisture content of the sprayed dissolving pulp board. According to the method provided by the invention, the reaction property of the dissolving pulp board is improved, meanwhile, not only is the waste of water resource avoided, but also the energy consumption is reduced, and the method is lower in cost.

Description

[0001] 【Technical field】 [0002] The invention relates to a method for improving the reaction performance of substances, in particular to a method for improving the reaction performance of dissolving pulp plates. [0003] 【Background technique】 [0004] Dissolving pulp is a special pulp in the pulp and paper industry. It is a refined pulp prepared by chemically treating plant fiber raw materials. Dissolving pulp has many characteristics, including high cellulose content, low lignin and other impurities, high brightness, and excellent reactivity. Dissolving pulp can produce regenerated cellulose, including viscose fiber, nitrocellulose and acetate cellulose, etc.; can prepare cellulose derivatives, including carboxymethyl cellulose, ethyl cellulose and methyl cellulose; can produce nanocellulose , including nanofibrillated cellulose and nanocrystalline cellulose. Therefore, dissolving pulp products and their derivatives have been widely used in many fields such as textiles, f...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21C5/00
CPCD21C5/005
Inventor 李建国欧阳新华苗庆显黄六莲陈礼辉倪永浩
Owner FUJIAN AGRI & FORESTRY UNIV
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