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A heat-conducting asphalt composite material, its preparation method and application

A technology of composite materials and thermal interface materials, applied in the field of thermal interface materials, can solve the problems of high cost of polymer matrix and low thermal conductivity of fillers, and achieve the effects of being suitable for large-scale production, improving softening point and mild conditions.

Active Publication Date: 2018-11-06
HUAZHONG UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The inorganic thermally conductive filler forms a network with high thermal conductivity in the SBS phase, and at the same time enhances the thermal properties of the SBS modified asphalt matrix and improves the softening point of the composite material, thereby solving the problem of low thermal conductivity of the filler in the prior art and high cost of the polymer matrix technical issues

Method used

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  • A heat-conducting asphalt composite material, its preparation method and application
  • A heat-conducting asphalt composite material, its preparation method and application
  • A heat-conducting asphalt composite material, its preparation method and application

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preparation example Construction

[0035] A method for preparing a heat-conducting asphalt composite material provided by the invention comprises the following steps:

[0036] (1) dissolving 8-16 parts by mass of styrene-butadiene-styrene block copolymer in 12-24 parts by mass of organic solvent to obtain a viscous solution;

[0037] (2) Mix 5 to 500 parts by mass of the inorganic thermally conductive filler with the obtained viscous solution, volatilize the solvent, and grind evenly to obtain a thermally conductive filler premix;

[0038] (3) fully mixing the heat-conducting filler premix with 100 parts by mass of base asphalt to obtain the primary material of the heat-conducting asphalt composite material;

[0039] (4) spreading and hot-pressing the heat-conducting asphalt composite primary material to obtain a heat-conducting asphalt composite material.

[0040] The organic solvent in step (1) is cyclohexane, methyl ethyl ketone, tetrahydrofuran, ethyl acetate, tetrachloroethylene or trichloroethylene.

[...

Embodiment 1

[0047] A thermally conductive bitumen composite comprising SBS 1301-1, alumina and No. 70 base bitumen. The alumina is selectively distributed in SBS 1301-1, based on 100 parts by mass of base asphalt, the addition amount of SBS 1301-1 is 9 parts, and the addition amount of alumina is 100 parts. The SBS 1301-1 has a linear structure, a molecular weight of 100,000-130,000, and an average polystyrene segment content of 30 wt%. The alumina is spherical, with an average particle size of 5 μm.

[0048] The preparation method of the heat-conducting asphalt composite material comprises the following steps:

[0049] (1) 9g of SBS 1301-1 was dissolved in 14g of tetrachlorethylene to obtain a viscous solution;

[0050] (2) Mix 100g of alumina with the obtained viscous solution evenly, place the mixture in an oven at 120°C to evaporate the solvent, and then grind it evenly to obtain a thermally conductive filler premix;

[0051] (3) Heat 100 g of base asphalt to 160° C., mix the heat-...

Embodiment 2

[0056] A thermally conductive bitumen composite comprising SBS 1301-1, alumina and No. 70 base bitumen. The alumina is selectively distributed in SBS 1301-1, based on 100 parts by mass of base asphalt, the addition amount of SBS 1301-1 is 9 parts, and the addition amount of alumina is 150 parts. The SBS 1301-1 has a linear structure, a molecular weight of 100,000-130,000, and an average polystyrene segment content of 30 wt%. The alumina is spherical, with an average particle size of 5 μm.

[0057] The preparation method of the heat-conducting asphalt composite material comprises the following steps:

[0058] (1) 9g of SBS 1301-1 was dissolved in 14g of tetrachlorethylene to obtain a viscous solution;

[0059] (2) Mix 150g of alumina with the obtained viscous solution evenly, place the mixture in an oven at 120°C to evaporate the solvent, and then grind it evenly to obtain a thermally conductive filler premix;

[0060] (3) Heat 100 g of base asphalt to 160° C., mix the heat-...

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Abstract

The invention discloses a heat conducting asphalt composite as well as a preparing method and an application thereof. The preparing method comprises the following steps: first, dissolving 8-16 parts by mass of a styrene-butadiene-styrene block copolymer in 12-24 parts of an organic solvent so as to obtain a thick solution; then, uniformly mixing 5-500 parts of a nonorganic heat conducting filler with the obtained thick solution, evaporating the solvent, and grinding even so as to obtain a heat conducting filler premix; fully mixing the heat conducting filler premix with 100 parts of matrix asphalt so as to obtain a heat conducting asphalt composite primary material; and finally paving and hot-pressing the heat conducting asphalt composite primary material so as to obtain the heat conducting asphalt composite. According to the heat conducting asphalt composite prepared by the method, the nonorganic heat conducting filler is selectively distributed in SBS phases, the heat conductivity and the thermal performance of the composite are obviously improved, and the heat conducting asphalt composite is particularly suitable for a thermal interface material. The preparing method provided by the invention is simple in technology, low in cost and suitable for massive production.

Description

technical field [0001] The invention belongs to the field of thermal interface materials, and more specifically relates to a heat-conducting asphalt composite material, its preparation method and application. Background technique [0002] With the rapid development of electronic technology, the integration and assembly density of electronic components are constantly increasing. While providing powerful functions, it also leads to a sharp increase in the heat generated during work. Timely and effective heat dissipation has become an urgent problem to be solved. . When the electronic components are in direct contact with the heat sink, due to the microscopic unevenness between the two solid contact surfaces, the actual contact area may only be 1% to 2% of the actual area, and the thermal conductivity of the air in the gap is only 0.025W m -1 ·K -1 , which results in a huge thermal resistance between the interfaces. Filling the thermal interface material with high thermal co...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L95/00C08L53/02C08K7/18C08K3/22C08K3/38C08K3/28C09K5/14
CPCC08K2201/003C08L95/00C08L2201/08C09K5/14C08L53/02C08K7/18C08K2003/2227C08K2003/385C08K2003/282
Inventor 解孝林文颖峰周兴平叶昀昇李晓静陈超
Owner HUAZHONG UNIV OF SCI & TECH
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