A heat-conducting asphalt composite material, its preparation method and application
A technology of composite materials and thermal interface materials, applied in the field of thermal interface materials, can solve the problems of high cost of polymer matrix and low thermal conductivity of fillers, and achieve the effects of being suitable for large-scale production, improving softening point and mild conditions.
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[0035] A method for preparing a heat-conducting asphalt composite material provided by the invention comprises the following steps:
[0036] (1) dissolving 8-16 parts by mass of styrene-butadiene-styrene block copolymer in 12-24 parts by mass of organic solvent to obtain a viscous solution;
[0037] (2) Mix 5 to 500 parts by mass of the inorganic thermally conductive filler with the obtained viscous solution, volatilize the solvent, and grind evenly to obtain a thermally conductive filler premix;
[0038] (3) fully mixing the heat-conducting filler premix with 100 parts by mass of base asphalt to obtain the primary material of the heat-conducting asphalt composite material;
[0039] (4) spreading and hot-pressing the heat-conducting asphalt composite primary material to obtain a heat-conducting asphalt composite material.
[0040] The organic solvent in step (1) is cyclohexane, methyl ethyl ketone, tetrahydrofuran, ethyl acetate, tetrachloroethylene or trichloroethylene.
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Embodiment 1
[0047] A thermally conductive bitumen composite comprising SBS 1301-1, alumina and No. 70 base bitumen. The alumina is selectively distributed in SBS 1301-1, based on 100 parts by mass of base asphalt, the addition amount of SBS 1301-1 is 9 parts, and the addition amount of alumina is 100 parts. The SBS 1301-1 has a linear structure, a molecular weight of 100,000-130,000, and an average polystyrene segment content of 30 wt%. The alumina is spherical, with an average particle size of 5 μm.
[0048] The preparation method of the heat-conducting asphalt composite material comprises the following steps:
[0049] (1) 9g of SBS 1301-1 was dissolved in 14g of tetrachlorethylene to obtain a viscous solution;
[0050] (2) Mix 100g of alumina with the obtained viscous solution evenly, place the mixture in an oven at 120°C to evaporate the solvent, and then grind it evenly to obtain a thermally conductive filler premix;
[0051] (3) Heat 100 g of base asphalt to 160° C., mix the heat-...
Embodiment 2
[0056] A thermally conductive bitumen composite comprising SBS 1301-1, alumina and No. 70 base bitumen. The alumina is selectively distributed in SBS 1301-1, based on 100 parts by mass of base asphalt, the addition amount of SBS 1301-1 is 9 parts, and the addition amount of alumina is 150 parts. The SBS 1301-1 has a linear structure, a molecular weight of 100,000-130,000, and an average polystyrene segment content of 30 wt%. The alumina is spherical, with an average particle size of 5 μm.
[0057] The preparation method of the heat-conducting asphalt composite material comprises the following steps:
[0058] (1) 9g of SBS 1301-1 was dissolved in 14g of tetrachlorethylene to obtain a viscous solution;
[0059] (2) Mix 150g of alumina with the obtained viscous solution evenly, place the mixture in an oven at 120°C to evaporate the solvent, and then grind it evenly to obtain a thermally conductive filler premix;
[0060] (3) Heat 100 g of base asphalt to 160° C., mix the heat-...
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Abstract
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