Modified foamed titanium particle electrode with electrocatalytic chlorophenol removing function and preparation method thereof
A particle electrode and titanium foam technology, which is applied in chemical instruments and methods, oxidized water/sewage treatment, water pollutants, etc., can solve the problems of short life, insufficient stability, and high cost of electrode materials
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[0059] (1) Wash 126g of foamed titanium particles with a particle size of 4-6mm with 1000mL of deionized water, then soak them in 500mL of chloroform for 8 hours, take them out, wash them with 1000mL of deionized water, and then wash them with 1000mL of 95% by mass. After washing with % ethanol, place it in a drying oven at 85°C for 1.5h to obtain substance A1;
[0060] (2) Add 8.27 grams of platinum nitrate and 750 mL of deionized water into a conical flask with a volume of 1000 mL, stir for 3 minutes at 1000 r / min, add 15 mL of concentrated nitric acid, shake well and divide into 3 equal parts to obtain a mixed solution K1, mixed solution K2, mixed solution K3;
[0061] (3) 820 mg Ce(NO 3 ) 3 and 50 mL of AgNO with a molar concentration of 0.42 mol / L 3 The solution was added to the mixed solution K1, and stirred at 1000r / min for 3 minutes to obtain the mixed solution L1;
[0062](4) Add substance A1 to the mixture L1, shake in a shaker at 45°C for 15 minutes, cool to roo...
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