Rosin processing method

A processing method and rosin technology, which are applied in the field of rosin production, can solve the problems of uneven color and low purity of rosin, and achieve the effects of good effect, high purity and light and uniform color.

Inactive Publication Date: 2017-04-26
临沧方源林产品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the rosin produced by the rosin processing method commonly used in industrial production is uneven in color and low in purity, so it is difficult to meet the increasing needs of industrialization and daily use

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A processing method of rosin, comprising the steps of:

[0023] (1) pine resin is pulverized, crosses 100 mesh sieves;

[0024] (2) 10kg of rosin after pulverization is transferred to a meterable reactor, drop into ethanol with 2 times of rosin volume, and 3% pimaric acid of rosin weight, at a stirring speed of 500r / min, heat to 60-80 ℃, keep warm for 45 minutes to fully melt;

[0025] (3) at 0.5-1.5kg / cm 2 Under the condition of steam pressure and temperature of 60-80°C, pass the melted rosin through the filter layer to remove coarse impurities to obtain filtrate;

[0026] (4) at 0.5-1.5kg / cm 2 Under the condition of steam pressure and temperature of 60-80°C, the filtrate in step (3) is further purified by tangential flow membrane separation technology to obtain the permeable membrane liquid; the tangential flow membrane adopts a flat plate made of inorganic ceramic material Membrane with a pore size of 200um;

[0027] (5) transfer the permeation solution to a ste...

Embodiment 2

[0030] A processing method of rosin, comprising the steps of:

[0031] (1) pine resin is pulverized, crosses 50 mesh sieves;

[0032] (2) 10kg of turpentine after pulverization is transferred to a meterable reactor, drop into turpentine with 3 times of turpentine volume, and abietic acid with 1% rosin weight, and heat to 60-80°C at a stirring speed of 800r / min , keep warm for 30 minutes to fully melt;

[0033] (3) at 0.5-1.5kg / cm 2 Under the condition of steam pressure and temperature of 60-80°C, pass the melted rosin through the filter layer to remove coarse impurities to obtain filtrate;

[0034] (4) at 0.5-1.5kg / cm 2 Under the condition of vapor pressure and temperature of 60-80°C, the filtrate in step (3) is further purified by tangential flow membrane separation technology to obtain permeable membrane liquid; the tangential flow membrane adopts organic material tubular membrane , the membrane pore size is 100um;

[0035] (5) transfer the permeation solution to a stea...

Embodiment 3

[0038] A processing method of rosin, comprising the steps of:

[0039] (1) pine resin is pulverized, crosses 100 mesh sieves;

[0040] (2) 10kg of rosin after pulverizing is transferred in a meterable reactor, drop into the rosin water equal to the volume of rosin, and the abietic acid of 5% rosin weight, under the stirring speed of 300r / min, be heated to 60- 80°C, keep warm for 60 minutes to fully melt;

[0041] (3) at 0.5-1.5kg / cm 2 Under the condition of steam pressure and temperature of 60-80°C, pass the melted rosin through the filter layer to remove coarse impurities to obtain filtrate;

[0042] (4) at 0.5-1.5kg / cm 2 Under the conditions of vapor pressure and temperature of 60-80°C, the filtrate in step (3) is further purified by tangential flow membrane separation technology to obtain the permeable membrane liquid; the tangential flow membrane adopts a roll type of inorganic ceramic material Membrane with a pore size of 500um;

[0043] (5) transfer the permeation s...

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Abstract

The invention relates to the technical field of rosin production, in particular to a rosin processing method. The rosin processing method specifically includes steps: smashing rosin; adding a solvent; melting, and roughly filtering; performing tangential flow film separation; distilling; cooling to obtain solid-state rosin. By adopting the rosin processing method, impurity ingredients in rosin can be removed effectively, and the obtained solid-state rosin is shallow and uniform in color and high in purity.

Description

technical field [0001] The invention relates to the technical field of rosin production, in particular to a processing method of rosin. Background technique [0002] Rosin is one of the most productive natural resins in nature. It has excellent physical and chemical properties and is an indispensable raw material for many industries such as papermaking, paint, ink, matches, rubber, electrical appliances, medicine, and textiles. Rosin is a non-volatile natural resin obtained from pine rosin through different processing methods. After the xylem of slash pine and masson pine is damaged, a lot of turpentine will flow out from the wound. These pine resins will be severely oxidized into yellow, brown or black solids during long-term contact with the air, and their physical and chemical properties are quite different from fresh rosin, and rosin is in the process of accumulating and gathering with many barks. Impurities and silt stick together and are difficult to remove. Rosin c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09F1/02C09F3/00
CPCC09F1/02C09F3/00
Inventor 方孔政
Owner 临沧方源林产品有限公司
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