Water-based aluminum silver slurry and preparation method thereof, as well as application of water-based aluminum silver slurry in ink
An aluminum-silver paste, water-based technology, used in inks, applications, chemical instruments and methods, etc., can solve the problems that limit the wide application of water-based aluminum-silver paste and the high volatile organic compounds, and achieve good gas stability, good stability, The effect of broadening the application field
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0025] The invention provides a kind of preparation method of water-based aluminum-silver paste, comprising the following steps:
[0026] a) mixing the oily aluminum silver paste with an alcoholic solvent, and separating the solid and liquid after ultrasonic dispersion to obtain a solid mixture;
[0027] b) mixing the solid mixture, alcohol solvent, pH regulator, silane coupling agent and ethyl orthosilicate, aging after reaction, and separating solid and liquid to obtain coated aluminum-silver paste;
[0028] c) drying the coated aluminum-silver paste to obtain aluminum-silver powder;
[0029] d) The aluminum-silver powder is mixed with a solvent and then separated from solid and liquid to obtain a water-based aluminum-silver paste.
[0030] In the preparation method provided by the present invention, the oily aluminum-silver paste is first washed with an alcohol solvent, and the fatty acid in the oily aluminum-silver paste is washed away, so that it can be better dispersed ...
Embodiment 1
[0054] (1) Take 100kg of the oily filter cake prepared by the preparation method in the application number CN201210467860.7, add 250kg of n-propanol, heat up to 50°C, turn on the ultrasound for 30min, stir for 2h and then separate the solid and liquid to obtain the filter cake;
[0055] (2) Place the filter cake washed in step (1) in the reactor, add 450kg of n-propanol, adjust the pH value of the solution to 8 with ammonia water, add vinyltriethoxysilane and ethyl orthosilicate dropwise Mix the solution for 2 hours, age for 6 hours, and separate the solid and liquid to obtain the coated aluminum paste;
[0056] (3) Place the aluminum paste coated in step (2) in an oven at 100°C, and bake in vacuum for 4 hours;
[0057] (4) the aluminum powder that step (3) is dried is passed through a 500-mesh vibrating sieve;
[0058] (5) Place the aluminum powder sieved in step (4) in a dispersing cylinder that fully meets the requirements of environmental protection, add 5 times of n-prop...
Embodiment 2
[0068] (1) Take 100 kg of the oily filter cake prepared by the preparation method in the application number CN201210467860.7, add 280 kg of n-propanol, heat up to 55° C., turn on the ultrasound for 50 minutes, and separate the solid and liquid after stirring for 2 hours to obtain the filter cake;
[0069] (2) Place the filter cake washed in step (1) in the reactor, add 550kg of n-propanol, adjust the pH value of the solution to 8 with ammonia water, add vinyltriethoxysilane and ethyl orthosilicate dropwise Mix the solution for 3 hours, age for 5 hours, and separate the solid and liquid to obtain the coated aluminum paste;
[0070] (3) Place the aluminum paste coated in step (2) in an oven at 100°C, and bake in vacuum for 5 hours;
[0071] (4) the aluminum powder that step (3) is dried is passed through a 500-mesh vibrating sieve;
[0072] (5) Place the aluminum powder sieved in step (4) in a dispersing cylinder that fully meets the requirements of environmental protection, ad...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com