Circulating production process for preparing hydrogen fluoride by utilizing fluorosilicic acid
A production process, fluosilicic acid technology, applied in the direction of fluorine/hydrogen fluoride, hydrogen fluoride, silicon oxide, etc., can solve the problems of high yield, low value of by-products, low cost, etc., and achieve the effect of high yield and low process cost
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[0039] Example 1
[0040] 1. The first production cycle
[0041] 1) Take 10 kg of fluorosilicic acid with a mass fraction of 20% and 0.73 kg of lithium fluoride solid to react in a still to obtain a mixed solution of hydrogen fluoride and lithium fluorosilicate;
[0042] 2) Vacuum distillation at 95 degrees Celsius for 1.5 hours in the reactor to distill out hydrogen fluoride gas to obtain lithium fluorosilicate solid;
[0043] 3) Take out the solid in step 2) and heat it to 450 degrees Celsius for 1.5 hours to obtain lithium fluoride solid and silicon tetrafluoride gas; absorb with 3.3 kg of 20% fluorosilicic acid solution to make the concentration of fluorosilicic acid solution Elevate and generate silica gel, filter silica gel, and reserve the fluorosilicic acid solution for later use;
[0044] 2. The second production cycle
[0045] 1) The fluorosilicic acid obtained after absorbing silicon tetrafluoride in step 3) of the first production cycle and the lithium fluoride obtained by t...
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[0051] Example 2
[0052] 1. The first production cycle
[0053] 1) Take 10 kg of fluorosilicic acid with a mass fraction of 15% and 1.27 kg of lithium fluoride solid to react in a still to obtain a suspension mixture of hydrogen fluoride, lithium fluorosilicate and the remaining excess lithium fluoride;
[0054] 2) Distill 1h at 180 degrees Celsius in the reactor to distill out hydrogen fluoride gas to obtain lithium fluorosilicate and lithium fluoride solids;
[0055] 3) Take out the solid in step 2) and heat it to 550 degrees Celsius for 1 hour to obtain lithium fluoride solid and silicon tetrafluoride gas; absorb with 3.3 kg of a 15% fluorosilicic acid solution to increase the concentration of the fluorosilicic acid solution High and generate silica gel, and the fluorosilicic acid solution is reserved for future use.
[0056] 2. The second production cycle
[0057] 1) In step 3) of the first production cycle, the fluorosilicic acid obtained after absorbing silicon tetrafluoride and ...
Example Embodiment
[0063] Example 3
[0064] 1. The first production cycle
[0065] 1) Take 10 kg of fluorosilicic acid with a mass fraction of 10% and 1.08 kg of lithium fluoride solid to react in a still to obtain a suspension mixture of hydrogen fluoride, lithium fluorosilicate and the remaining excess lithium fluoride;
[0066] 2) Distill in the reactor at 150 degrees Celsius for 2 hours to distill out hydrogen fluoride gas to obtain a solid mixture of lithium fluorosilicate and lithium fluoride;
[0067] 3) Take out the solid in step 2) and heat it to 300 degrees Celsius for 3 hours to obtain lithium fluoride solid and silicon tetrafluoride gas; absorb with 3.3kg of 10% fluorosilicic acid solution to increase the concentration of fluorosilicic acid solution High and generate silica gel, and the fluorosilicic acid solution is reserved for future use.
[0068] 2. The second production cycle
[0069] 1) In the first production cycle step 3), the fluorosilicic acid obtained after absorbing silicon tetraf...
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