Application of high-positive-charge green fluorescent protein in preparing liver cancer early diagnostic kit
A green fluorescent protein, high positive charge technology, applied in the field of medicine and cell biology, can solve the problems affecting the specificity of HCC diagnosis, missed tumor detection, etc., and achieve the effect of saving measurement time, simple steps, and reducing the amount of use
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Embodiment 1
[0029] Example 1. Detection of different concentrations of GPC3 in PBS with highly positive green fluorescent protein.
[0030] 60 μL of GPC3 antibody (purchased from Abcam, 30 ng / mL) was spread on a 384 microwell white plate and blocked with 1% BSA. After blocking, wash with PBS 3 times, then add different concentrations of GPC3 and GPC3ΔGAG (GPC3 without glycosaminoglycan side chains) dissolved in PBS, leave at room temperature for 2 hours, after incubation, wash 3 times with PBS, add 0.3 μg of highly positively charged green fluorescent protein (ScGFP), placed at room temperature in the dark for 10 min, washed 5 times with PBS, and measured for fluorescence intensity (Ex: 470nm, Em: 509nm). The results showed that as the content of GPC3 and GPC3ΔGAG increased, the fluorescence intensity also increased; at the same concentration, the ability of GPC3 to bind fluorescence was stronger than that of GPC3ΔGAG (such as figure 1 shown). This shows that the glycosaminoglycan side...
Embodiment 2
[0031] Example 2. Detection of different concentrations of GPC3 in serum with highly positive green fluorescent protein.
[0032] As mentioned above, the specific antibody of GPC3 was plated in 384 microwell white plates and blocked. Then add GPC3 and GPC3ΔGAG dissolved in appropriately diluted fetal bovine serum, and place at room temperature for 2 hours. After incubation, wash 3 times with PBS, add 0.3 μg ScGFP, place in the dark at room temperature for 10 minutes, wash 5 times with PBS, and measure the fluorescence intensity (Ex: 470nm, Em: 509nm). The results showed that as the content of GPC3 and GPC3ΔGAG increased, the fluorescence intensity also increased; at the same concentration, GPC3 had a stronger ability to bind fluorescence than GPC3ΔGAG; but it was less sensitive than in PBS (such as figure 2 shown). This shows that the high-positive green fluorescent protein can detect GPC3 in serum, which provides a simple and quick method for the early diagnosis of liver c...
Embodiment 3
[0033] Embodiment 3, the impact of salt concentration on the detection of GPC3 in serum
[0034] Add different concentrations of NaCl to fetal bovine serum containing GPC3, incubate at 30° C. for 1 hour with occasional gentle shaking, and then detect the effect of salt concentration on the detection of GPC3 in serum by the method in Example 2. The results show that compared with no NaCl, 0.5M NaCl can significantly improve the fluorescence intensity of the detection sample (such as image 3 shown).
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