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Method for preparing pregelatinized starch from sweet potato starch

A technology of pregelatinized starch and sweet potato starch, which is applied in the field of preparing pregelatinized starch from sweet potato starch, can solve the problems of crystal structure destruction, mechanical activation method and chemical method can not fully meet the activation requirements, etc., and achieve the purpose of inhibiting swelling and drying Thorough, good solubility effect

Inactive Publication Date: 2017-09-15
ANHUI ZISHAN AGRI TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The process of starch pregelatinization is divided into mechanical activation and chemical activation. Traditionally, mechanical activation is commonly used. Mechanical activation is achieved by ball milling. Ball milling uses the impact of balls to mechanically activate and pulverize materials. Traditional ball milling The method is to use zirconia as the ball milling medium. After the ball milling, the crystal structure of the starch is destroyed, changing from a polycrystalline structure to an amorphous structure. At the same time, it also causes changes in the molecular chain arrangement and molecular weight arrangement of the starch, which leads to starch modification, and then changes The gelatinization and rheological properties of starch, etc., but a single mechanical activation method and chemical method sometimes cannot fully meet the activation requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A method for preparing pregelatinized starch with sweet potato starch, comprises the steps:

[0023] Step 1: Add sweet potato starch and ethanol solution with a mass ratio of 1:5 in the ball mill barrel of the mechanical activation device, stir for 10min under the action of a stirrer at 500rmp, the stirring temperature is 40°C and then put the stirred mixture at 60°C Carry out drying, obtain primary activated starch;

[0024] Step 2: Grinding and sieving the primary activated starch prepared in step 1 to obtain 60-100 mesh starch granules, and then adding the primary activated starch, silicone oil, sodium alginate and water to the mixer at a mass ratio of 1:0.01:0.1:50 , stirring in a stirrer with a speed of 1000rmp for 10min and a stirring temperature of 60°C to obtain a secondary activated starch;

[0025] Step 3: Add sodium bicarbonate to the secondary activated starch prepared in step 2, wherein the mass ratio of the secondary activated starch to sodium bicarbonate...

Embodiment 2

[0028] A method for preparing pregelatinized starch with sweet potato starch, comprises the steps:

[0029] Step 1: Add sweet potato starch and ethanol solution with a mass ratio of 1:15 in the ball mill barrel of the mechanical activation device, stir for 20min under the action of an agitator at 800rmp, and the stirring temperature is 60°C and then put the stirred mixture at 70°C Carry out drying, obtain primary activated starch;

[0030] Step 2: crush and sieve the preliminary activated starch prepared in step 1 to obtain 60-100 mesh starch granules, then mix primary activated starch, silicone oil, sorbitan fatty acid ester and water with a ratio of 1:0.1:0.5:100 Put the mass ratio into the mixer, stir in the mixer at a speed of 1500rmp for 20min, and the stirring temperature is 60°C to obtain the secondary activated starch;

[0031] Step 3: Add sodium bicarbonate to the secondary activated starch prepared in step 2, wherein the mass ratio of secondary activated starch to s...

Embodiment 3

[0034] A method for preparing pregelatinized starch with sweet potato starch, comprises the steps:

[0035] Step 1: Add sweet potato starch and ethanol solution with a mass ratio of 1:20 in the ball mill barrel of the mechanical activation device, stir for 30min under the action of a stirrer at 1000rmp, the stirring temperature is 70°C and then put the stirred mixture at 80°C Carry out drying, obtain primary activated starch;

[0036] Step 2: Grinding and sieving the primary activated starch prepared in step 1 to obtain 60-100 mesh starch granules, and then adding the primary activated starch, edible oil, carrageenan and water to the mixer at a mass ratio of 1:0.5:0.9:200 , stirring in a stirrer at a speed of 2000rmp for 50min at a stirring temperature of 80°C to obtain a secondary activated starch;

[0037] Step 3: Add sodium bicarbonate to the secondary activated starch prepared in step 2, wherein the mass ratio of the secondary activated starch to sodium bicarbonate is 1:0...

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PUM

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Abstract

The invention discloses a method for preparing pregelatinized starch from sweet potato starch. The method is characterized by comprising the following steps: step 1, adding a certain amount of sweet potato starch and an ethyl alcohol solution into a ball milling barrel, carrying out mixing under stirring and then carrying out drying so as to obtain preliminarily activated starch; step 2, subjecting the preliminarily activated starch prepared in the step 1 to crushing and sieving and then mixing the preliminarily activated starch, a functional aid, a surfactant and water under stirring so as to obtain secondarily activated starch; step 3, adding sodium bicarbonate into the secondarily activated starch prepared in the step 2 and carrying out a stirring reaction so as to obtain pregelatinized starch; and step 4, subjecting the pregelatinized starch prepared in the step 3 to microwave drying in a microwave drying machine and crushing the dried pregelatinized starch with a pulverizer so as to obtain a final product. According to the method in the invention, ethanol is used as a medium, preliminary activation is carried out on the starch by using a mechanical activation method, and then chemical activation is carried out, so the process of activation is more thorough.

Description

technical field [0001] The invention belongs to the field of pregelatinized starch preparation and relates to a method for preparing pregelatinized starch from sweet potato starch. Background technique [0002] The process of starch pregelatinization is divided into mechanical activation and chemical activation. Traditionally, mechanical activation is commonly used. Mechanical activation is achieved by ball milling. Ball milling uses the impact of balls to mechanically activate and pulverize materials. Traditional ball milling The method is to use zirconia as the ball milling medium. After the ball milling, the crystal structure of the starch is destroyed, changing from a polycrystalline structure to an amorphous structure. At the same time, it also causes changes in the molecular chain arrangement and molecular weight arrangement of the starch, which leads to starch modification, and then changes The gelatinization and rheological properties of starch, etc., but a single me...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08B30/14C08B30/02C08B30/06
CPCC08B30/14C08B30/02C08B30/06
Inventor 范子山范冰
Owner ANHUI ZISHAN AGRI TECH CO LTD
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