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Sodium acrylate water-absorbing swelling resin solution, PET fiber water-absorbing swelling water-blocking tape and preparation method thereof

A water-absorbent resin, sodium acrylate technology, applied in the direction of fiber processing, fiber type, fiber mechanical structure, etc., can solve the problems of affecting the manufacturing cost of optical cables, low swelling water absorption performance, etc., and achieves rapid copolymerization and crosslinking. Lightweight effect

Active Publication Date: 2019-11-26
岳阳澳源通信材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, its swelling and water absorption thickness (5min) is less than 10mm, and the expansion and water absorption performance is lower than the industry standard.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0018] Hereinafter, the present invention will be further described in conjunction with the embodiments.

[0019] (1) Preparation of sodium acrylate water-absorbing resin solution:

[0020] Inject 20-100 parts of deionized water into the water-cooled reactor;

[0021] Fill the water-cooled reaction kettle with 5-60 parts of sodium hydroxide, 3 times within 1 hour, and 10 parts each time. The temperature is cooled to 35 ℃ under water cooling;

[0022] Fill the water-cooled reaction kettle with 4-40 parts of acrylic acid. The continuous filling is completed within 1 hour. The water-cooling temperature should be controlled at 35 ℃, and the PH value should be controlled at 6.5;

[0023] Mix 2-20 parts of acrylamide with 5-50 parts of deionized water to prepare an aqueous solution of acrylamide; then add the aqueous solution of acrylamide to a water-cooled reactor and stir for 10 minutes;

[0024] Add 0.5-10 parts of ammonium persulfate and 1-7 parts of potassium persulfate, and stir for 10 m...

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Abstract

A sodium acrylate water-absorbing resin solution, its composition (by weight) is: 20-100 parts of deionized water, 5-60 parts of sodium hydroxide, 4-40 parts of acrylic acid, 2-20 parts of acrylamide, 1-20 parts of potassium persulfate 7 parts, 0.5-10 parts of ammonium persulfate, 0.1-6 parts of N-(hydroxymethyl)acrylamide. The sodium acrylate water-absorbing resin solution provided by the present invention contains two initiators, ammonium persulfate and potassium persulfate, which can slow down the crosslinking speed during the copolymerization and crosslinking reaction, and weaken the influence of the high temperature generated by the exothermic reaction on the copolymerization rate. Reduce heat release. The preparation method is as follows: neutralize the sodium hydroxide aqueous solution and acrylic acid, then add the acrylamide aqueous solution, ammonium persulfate, potassium persulfate and N-(hydroxymethyl)acrylamide in sequence, and slow release after stirring. The present invention also includes a PET fiber water-absorbing swelling water-blocking tape prepared by using the sodium acrylate water-absorbing resin solution. The PET fiber water-absorbing swelling water-blocking tape prepared by the method is light in weight per square meter, soft in texture, high in swelling thickness and It expands quickly and blocks water in the optical cable, and has good water blocking effect.

Description

Technical field [0001] The invention relates to the field of water-blocking material manufacturing, in particular to a sodium acrylate water-absorbing resin solution, a water-absorbing swelling water-blocking tape and a preparation method thereof. Background technique [0002] The structure of the communication optical cable directly affects the user experience, and the selection of the water blocking material of the optical cable has an impact on the quality of its structure. Currently, most of the materials used in the water-blocking process in the optical cable structure are: 1. Grease-type water-blocking fiber paste and cable paste; 2. Non-woven fabric adhesive sodium acrylate water-absorbing resin composite water-blocking tape. [0003] The oil-type water-blocking paste is added to the optical cable, which is used in large quantities in production, and the production of oil pollutes the environment and consumes a lot of petroleum resources. In addition, the optical cable proc...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08F220/06C08F220/56D06M15/263G02B6/44D06M101/32
CPCD06M15/263C08F220/06D06M2101/32G02B6/44384C08F220/56
Inventor 罗雄
Owner 岳阳澳源通信材料有限公司