Direct oral decoction pieces of Chinese medicine of sunset abelmoschus flower powder
A technology for decoction pieces of traditional Chinese medicine and hollyhocks, which is applied in the field of medicine and can solve problems such as damage to chemical properties, complex chemical components, and nuclear material residues.
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[0059] Preparation of reference substance solution Take an appropriate amount of hyperin reference substance, weigh it accurately, add methanol to make a solution containing 0.1mg per 1ml, and obtain it.
[0060] Preparation of the test solution Take about 0.5g of the fine powder of this product, weigh it accurately, put it in a stoppered conical flask, add 50ml of methanol accurately, weigh it, heat it under reflux for 1 hour, let it cool, weigh it again, and use Make up the lost weight with methanol, shake well, filter, and take the subsequent filtrate, that is, the obtained product.
[0061] Determination method Accurately draw the reference substance solution and the test solution respectively 10μl, inject the liquid chromatograph, measure, that is.
[0062] This product is calculated as a dry product, containing hyperin (H 21 h 20 o 12 ) shall not be less than 0.50%.
[0063] The polysaccharide content of the marshmallow flower was measured according to the determinat...
Embodiment 1
[0077] 120 kilograms of raw medicinal materials of hollyhock flower were divided into 3 experimental batches (40.0 kilograms per batch), which were purified, dried and crushed according to the drug GMP standard (D-level clean area, dust-absorbing low-temperature crushing technology was used, and crushed separately) into 80, 100, 120 mesh), intermediate (inspection), quantitative packaging (3 g / bag, D-level clean area), electron beam irradiation sterilization (30% of the remaining quantitative packaging in each batch is not sterilized operation), the resulting product (test sample) is used for the best GMP production process of hollyhock pollen of the present invention and its quality standard experimental research.
[0078] 1. The optimal production process of "Hullhock pollen" directly orally in Chinese herbal medicine:
[0079] (1) Optimum fineness (mesh number) production process:
[0080] The size of the rhizome cells of the hollyhock flower is more than ten to tens of mi...
PUM
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