Preparation method of environment-friendly polyimide insulating composite with high temperature resistance
An insulating composite material, polyimide technology, applied in the direction of synthetic cellulose/non-cellulose material pulp/paper, insulators, organic insulators, etc., can solve the impact of product dielectric properties, low online concentration, high product uniformity problems, to achieve the effect of improving the uniformity of the tissue structure, avoiding the influence, and reducing the difficulty of processing
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Embodiment 1
[0022] Example 1, a preparation method of an environment-friendly polyimide high temperature resistant insulating composite material:
[0023] (1) Disperse polyimide fibers in a fiber discrete device to obtain a suspension containing polyimide chopped fibers, and dilute with water;
[0024] (2) Use a beater to beat the pulp, then add it to the suspension containing chopped fibers, and mix evenly to obtain a pulp suspension;
[0025] (3) The slurry suspension is formed by a wet process on an inclined wire former to obtain an intermediate product of polyimide high temperature resistant insulating composite material;
[0026] (4) The intermediate product is subjected to hot-pressing treatment, and after cooling, the finished product of polyimide high-temperature-resistant insulating composite material is obtained;
Embodiment 2
[0027] Embodiment 2, a preparation method of an environment-friendly polyimide high temperature resistant insulating composite material: comprising the following steps:
[0028] (1) Disperse polyimide fibers in a fiber discrete device to obtain a suspension containing polyimide chopped fibers, which is diluted with water; the length of the chopped fibers is 3 mm; the concentration of the suspension is 0.5 wt‰;
[0029] (2) Use a beater to beat the pulp, then add it to the suspension containing chopped fibers, and mix evenly to obtain a slurry suspension; the pulp is a mixture of aramid pulp and sulfonamide pulp Composition, the mass ratio of the two is 1:2; the concentration of the beating is 0.1%, and the beating time is 5 min; the mixing time of the suspension and the pulp is 0.5 h; the mass percentage of chopped fibers in the pulp suspension 60%;
[0030] (3) The slurry suspension is formed by a wet process on an inclined wire former to obtain an intermediate product of p...
Embodiment 3
[0032] Embodiment 3, a preparation method of an environment-friendly polyimide high temperature resistant insulating composite material: comprising the following steps:
[0033] (1) Disperse polyimide fibers in a fiber discrete device to obtain a suspension containing polyimide chopped fibers and dilute with water; the length of the chopped fibers is 10mm; the concentration of the suspension is 6wt ‰;
[0034] (2) Use a beater to beat the pulp, then add it to the suspension containing chopped fibers, and mix evenly to obtain a slurry suspension; the pulp is aramid pulp and polyimide pulp It is made by mixing, the mass ratio of the two is 2:1; the concentration of the beating is 0.8%, and the beating time is 100min; the mixing time of the suspension and pulp is 4h; the mass percentage of chopped fibers in the pulp suspension 95%.
[0035] (3) The slurry suspension is formed by a wet process on an inclined wire former to obtain an intermediate product of polyimide high tempera...
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