Natural plant essential oil microcapsule as well as preparation method and application thereof
A technology of natural plant essential oil and plant essential oil, applied in the field of natural plant essential oil microcapsules and preparation, can solve the problems of easy volatility, small molecular weight of plant essential oil, short effective duration, etc. The effect of repellent time
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[0030] Example 1 Preparation of natural plant essential oil microcapsules by β-cyclodextrin
[0031] 1) Preparation of capsule core:
[0032] The essential oil compound includes the components in parts by weight as shown in Table 1, and weighs accordingly;
[0033] Table 1 The weight ratio of each component
[0034] Serial number
[0035] First disperse the first six components in soybean oil, then add the synergist lavender essential oil and cinnamon essential oil, and slowly heat to 50-70°C until it becomes transparent and clear. According to a certain proportion, put the formulated essential oil compound into a beaker , Add while stirring. After stirring evenly, let it cool naturally to obtain the synergistic compound, namely the oil phase;
[0036] Prepare capsule core liquid by mixing 5ml oil phase and 5ml ethanol;
[0037] 2) Preparation of the cyst wall
[0038] Weigh 5g of β-cyclodextrin, add 200ml of distilled water and stir evenly, heat in a water bath at 60°C to completely ...
Example Embodiment
[0043] Example 2 Preparation of natural plant essential oil microcapsules from urea-formaldehyde resin
[0044] 1) Preparation of capsule core:
[0045] The essential oil compound includes the components in parts by weight as shown in Table 2, and weighs accordingly;
[0046] Table 2 Weight ratio of each component
[0047] Serial number
[0048] First disperse the first six components in soybean oil, then add the synergist lavender essential oil and cinnamon essential oil, and slowly heat to 50-70°C until it becomes transparent and clear. According to a certain proportion, put the formulated essential oil compound into a beaker , Add while stirring. After stirring evenly, let it cool naturally to obtain the synergistic compound, namely the oil phase;
[0049] Mix 5ml oil phase and 5ml dichloromethane to obtain capsule core liquid;
[0050] 2) Preparation of the cyst wall
[0051] Weigh 10ml of urea-formaldehyde resin and add it to 50ml of water, add 2ml of Tween 80 and 2ml of Span 80 ...
Example Embodiment
[0056] Example 3 Preparation of natural plant essential oil microcapsules from gelatin-gum arabic
[0057] 1) Preparation of capsule core:
[0058] The essential oil compound includes the components in parts by weight as shown in Table 3, and weighs accordingly;
[0059] Table 3 Weight ratio of each component
[0060] Serial number
[0061] First disperse the first six components in soybean oil, then add the synergist lavender essential oil and cinnamon essential oil, and slowly heat to 50-70°C until it is transparent and clear. According to a certain proportion, put the formulated essential oil compound into a beaker , Add while stirring. After stirring evenly, let it cool naturally to obtain the synergistic compound, namely the oil phase;
[0062] Mix 5ml oil phase and 5ml dichloromethane to obtain capsule core liquid;
[0063] 2) Capsule wall and microencapsulation
[0064] In a 40°C water bath, measure 2ml of the capsule core liquid from step 1) and slowly add it to 40ml of gelati...
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