Perovskite film preparing method based on magnetic field regulation
A technology of magnetic field regulation and perovskite, which is applied in semiconductor/solid-state device manufacturing, electrical components, electric solid-state devices, etc., can solve problems such as the negative impact on the human body environment, achieve improved short-circuit current and conversion efficiency, smooth and dense surface, and electronic The effect of high extraction efficiency
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[0039] (1) Prepare the reaction solution
[0040] The specific method of configuration is to measure 2305mg of PbI 2 Drugs, 795mg MAI and 0.8ml dimethylsulfoxide (Dimethylsulfoxide, DMSO) were mixed into 4.2ml of dimethylformamide (N,N-Dimethylformamide, DMF). Then stirred at 70°C for 30min until the PbI 2 and MAI were completely dissolved to obtain the mixed solution to be tested.
[0041] (2) Adjustable growth of perovskite film
[0042] 1) Dense TiO has been formed on the heating surface in sequence 2 layer and mesoporous TiO 2 layer of FTO conductive glass substrate, so that its temperature is maintained at 140 °C.
[0043] 2) Install a rotating magnetic field device on the sample in step 1), and adjust its rotation speed to 1200 rpm and magnetic field size to 100 mt.
[0044] 3) Add the mixed solution prepared in step (1) dropwise on the sample prepared in the above 1), the dropping amount is 12 μl, scrape the mixed solution at a scraping speed of 2.5 cm / s, and then...
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