A kind of preparation method of wax for paper packaging material
A technology for packaging materials and raw materials, which is applied in petroleum wax refining, petroleum wax recycling, wax physical treatment, etc., can solve the problems of decreased product yield, prolonged sweating time, and low product yield.
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Embodiment 1
[0054] This embodiment includes two parts: (A) emulsification and (B) sweating.
[0055] (A) emulsification
[0056] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0057](A1) Oil phase material preparation
[0058] take 58 # Semi-refined wax (Sinopec Gaoqiao Branch, melting point 59.1°C, oil content 1.52%, sticking point temperature 35.7°C) 78.0Kg, heat to 75°C and add 2.0Kg of sorbitan monostearate, diethyl Diol monolaurate 0.9Kg and lauryl betaine 0.7Kg, stir well.
[0059] (A2) Preparation of aqueous phase materials
[0060] 0.15Kg of CO at 20.1 to 20.3 atmospheres 2 Dissolve in 18.25Kg of water and heat to 80°C.
[0061] (A3) Emulsion preparation
[0062] Pressurize the oil-phase material to 20.1-20.3 atmospheres, and stir at a speed of 600r / min; add the water-phase material prepared in (A2) to the oil-phase material prepared in (A1), and continue stirring for 25 minutes to form...
Embodiment 2
[0079] This embodiment includes two parts: (A) emulsification and (B) sweating.
[0080] (A) emulsification
[0081] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0082] (A1) Oil phase material preparation
[0083] take 58 # Semi-refined wax (same as Example 1) 81.0Kg, heated to 80°C and melted, added 2.6Kg of sorbitan monooleate, 1.0Kg of sorbitan monolaurate and 0.6Kg of triacetamide oleate, Stir well.
[0084] (A2) Preparation of aqueous phase materials
[0085] With 27.5% H 2 o 2 solution, solid KOH and H 2 O formulated with H 2 o 2 0.6%, KOH 2.5 mg / Kg aqueous solution, take 14.8Kg, pressurize to 22.8-23.0 atmospheres under nitrogen condition, and heat to 85°C.
[0086] (A3) Emulsion preparation
[0087] Pressurize the oil phase material to 22.8-23.0 atmospheres under nitrogen, and stir at a speed of 300r / min; add the water phase material prepared in (A2) to the oil phase ...
Embodiment 3
[0093] This embodiment includes two parts: (A) emulsification and (B) sweating.
[0094] (A) emulsification
[0095] This part includes (A1) oil phase material preparation, (A2) water phase material preparation, (A3) emulsion preparation three steps.
[0096] (A1) Oil phase material preparation
[0097] take 58 # Semi-refined wax (same as Example 1) 82.5Kg, heated to 71°C and melted, then added 2.0Kg of sorbitan monostearate, 0.5Kg of sorbitan monopalmitate and 0.3 Kg of sodium oleamide carboxylate , stir well.
[0098] (A2) Preparation of aqueous phase materials
[0099] With 27.5% H 2 o 2 solution, solid NaOH and H 2 O formulated with H 2 o 2 1.6%, NaOH 6.6 mg / Kg aqueous solution, take 14.7Kg, pressurize to 28.5-28.7 atmospheric pressure under nitrogen condition, and heat to 78°C.
[0100] (A3) Emulsion preparation
[0101] Pressurize the oil phase material to 28.5-28.7 atmospheres under nitrogen, and stir at a speed of 400r / min; add the water phase material prep...
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Abstract
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