Hot-pressing method for processing large-size super-hydrophobic cylindrical array capable of bouncing in droplet and cake shape

一种加工方法、超疏水的技术,应用在使原料颗粒化的方法、化学仪器和方法、图纹面的照相制版工艺等方向,能够解决难以实现产业化大面积加工、电火花加工效率低、高径比大等问题,达到易加工、密度小、高径比低的效果

Active Publication Date: 2018-01-12
DALIAN UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The superhydrophobic cone and square column arrays developed by Liu et al. have a diameter of about 20 μm to 100 μm and a height of about 800 μm to 1200 μm. Due to the small diameter and high aspect ratio of this type of structure, currently only the wire electric discharge method can be used. processed out
However, the efficiency of EDM is too low, and it takes 7 to 8 hours to process a 2cm×2cm sample, making it difficult to realize industrialized large-scale processing

Method used

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  • Hot-pressing method for processing large-size super-hydrophobic cylindrical array capable of bouncing in droplet and cake shape
  • Hot-pressing method for processing large-size super-hydrophobic cylindrical array capable of bouncing in droplet and cake shape
  • Hot-pressing method for processing large-size super-hydrophobic cylindrical array capable of bouncing in droplet and cake shape

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Experimental program
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Embodiment

[0024] A superhydrophobic cylinder array that can realize droplet cake-like bouncing can be processed by hot-pressing replication method of porous array template, such as figure 1 As shown, the specific method is as follows:

[0025] (1) Preparation of hot-pressing mold: Grinding with 800# and 1500# sandpaper and ultrasonically cleaning 6061 aluminum plate (thickness 1mm) with deionized water to remove surface oxide layer and oil stain; use drilling technology to process diameter 1.05mm, column spacing 0.25mm, 1.0mm deep array through-hole structure, use 1500# sandpaper to remove surface burrs, and then blow dry after ultrasonic cleaning with deionized water;

[0026] (2) Hot pressing: Place the array through-hole mold prepared in step 1 on the lower substrate of the press, then fix the PP material on the upper pressing plate, then adjust the temperature of the substrate to 180°C, adjust the pressure to 2000Pa, and heat for 10 minutes Then remove the pressure, take out the mo...

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Abstract

Provided is a hot-pressing method for processing a large-size super-hydrophobic cylindrical array capable of bouncing in a droplet and cake shape. The method comprises the steps of: preparing a hot-pressing mold, wherein a metal substrate array through-hole structure which has a diameter of 0.8-1.25 mm, column spacing of 0.25 mm, a depth of 0.6-1.0 mm is processed, grinding, washing and blow-drying are conducted on the metal substrate array through-hole structure to obtain the hot-pressing mold; conducting hot pressing, wherein a polymer material is applied to the hot-pressing mold, vacuum hotpressing is conducted on the hot-pressing mold with the polymer material, and the hot-pressing mold with the polymer material is cooled to a room temperature after taken out; removing the mold, wherein after the excessive polymer material flowing out of through holes is cut off, the hot-pressing mold is removed, and a polymer cylindrical array can be obtained; and conducting super-hydrophobic treatment, wherein the obtained cylindrical array is sprayed with a mixed solution to obtain the super-hydrophobic cylindrical array, and the mixed solution is a fluorosilane ethanol solution which contains nano TiO2 particles. The method has the advantages of being simple and easy to operate and low in cost, multiple kinds of materials can be selected, the materials and templates can be reused, andthe size of the prepared cylindrical array is large; besides, industrial processing and large surface of the super-hydrophobic cylindrical array capable of bouncing in the droplet and cake shape canbe effectively realized.

Description

technical field [0001] The invention belongs to the technical field of micromachining, and relates to a hot-pressing processing method of a large-size super-hydrophobic cylinder array capable of realizing liquid drop cake-like bouncing. Background technique [0002] Freezing rain is a common phenomenon in nature, but it is very easy to adhere to solid surfaces to freeze and cause damage to human production and life. For example, freezing rain attached to transmission lines can easily cause power outages; freezing rain attached to roads can easily reduce the friction between pedestrians and cars. Increase traffic accidents; freezing rain attached to the wings will reduce the lift of the aircraft and increase flight resistance, and serious crashes will also occur. The harm of freezing rain forces people to find effective ways to reduce its adhesion to solid surfaces. The superhydrophobic surface has attracted the attention of researchers due to its high contact angle and low ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J7/06B29C33/38B29C51/00
CPCB29C37/0003B29C37/0053B29C2059/023B29K2995/0093B29L2031/756B29C48/155B29C48/345B01J2/30B29C33/38B29C51/00B29C59/022G03F7/0002
Inventor 宋金龙黄柳赵长林高明谦刘新
Owner DALIAN UNIV OF TECH
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