Preparation method and application of three-dimensional multi-dimension porous crystal titanium carbide
A titanium carbide, multi-size technology, applied in the direction of titanium carbide, carbide, electrical components, etc., can solve the problems of easy stacking of two-dimensional crystal titanium carbide, low mass capacitance, etc., and achieve abundant reserves, high safety, and low price. Effect
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specific Embodiment approach 1
[0039] Specific implementation mode 1: This implementation mode is a preparation method of three-dimensional multi-size pore crystal titanium carbide, which is specifically completed according to the following steps:
[0040] 1. Preparation of two-dimensional layered titanium carbide nanosheets:
[0041] ①. Add lithium fluoride to hydrochloric acid with a concentration of 6mol / L-12mol / L, and then magnetically stir for 5min-10min at a stirring speed of 300r / min-500r / min to obtain solution A;
[0042] The volume ratio of the mass of lithium fluoride described in step 1. to concentration of hydrochloric acid of 6mol / L~12mol / L is (1g~3g):20mL;
[0043] ②. Add Ti to solution A in 3 to 15 times under the conditions of ice water bath and stirring speed of 200r / min to 1000r / min 3 AlC 2 powder, stirred to Ti 3 AlC 2 Disperse the powder evenly in solution A, then magnetically stir for 24h-72h at a temperature of 30°C-50°C and a stirring speed of 100r / min-500r / min to obtain solution ...
specific Embodiment approach 2
[0065] Specific embodiment two: the difference between this embodiment and specific embodiment one is: the mass of lithium fluoride described in step one ① and the volume ratio of the hydrochloric acid that concentration is 6mol / L~12mol / L are (1g~1.5g ): 20mL. Other steps are the same as in the first embodiment.
specific Embodiment approach 3
[0066] Specific embodiment three: the difference between this embodiment and specific embodiment one or two is: the mass of lithium fluoride described in step 1. and the concentration are 6mol / L~12mol / L The volume ratio of hydrochloric acid is ( 1.5g~3g): 20mL. Other steps are the same as those in Embodiment 1 or 2.
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