Method for preparing silver nanoparticles through caulis sargentodoxae extracting solution
A technology of silver nanoparticles and extracting solution, applied in the field of materials science, can solve the problems of easily polluting the environment, cumbersome processes, etc., and achieves the effects of environmental friendliness, simple preparation process, and no residue of chemical reagents
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Embodiment 1
[0026] (1) Rinse the used glass container with deionized water;
[0027] (2) Take 30mL red vine extract and put it into a flask, heat to boiling, and boil for 10 minutes;
[0028] (3) Add 1mL silver nitrate solution into the flask, test the pH value to 6.0, react under boiling conditions for 1 minute, 2 minutes, 3 minutes, 4 minutes, 5 minutes and then take samples;
[0029] (4) The samples obtained after the above different reaction times were centrifuged at 8000 rpm for 10 minutes, and the obtained precipitate was dried at 40-50°C for 10 minutes to obtain silver nanoparticles.
[0030] figure 2 The ultraviolet-visible absorption spectrum (UV-Vis) chart obtained by testing the reaction solution obtained from the above reaction for 1 minute, 2 minutes, 3 minutes, 4 minutes, and 5 minutes using a UV-2600 ultraviolet spectrophotometer from Shimadzu Corporation of Japan . The absorption peaks produced by silver nanoparticles are all around 430nm, and produce obvious plasmon r...
Embodiment 2
[0034] (1) Rinse the used glass container with deionized water;
[0035] (2) Take 30mL red vine extract and put it into a flask, heat to boiling, and boil for 10 minutes;
[0036] (3) Add 1.5mL silver nitrate solution into the flask, test the pH value to 5.7, react under boiling conditions for 1 minute, 2 minutes, 3 minutes, 4 minutes, 5 minutes and then take samples;
[0037] (4) The samples obtained after the above different reaction times were centrifuged at 8000 rpm for 10 minutes, and the obtained precipitate was dried at 40-50°C for 10 minutes to obtain silver nanoparticles.
[0038] Image 6 It is the ultraviolet-visible absorption spectrum (UV-Vis) chart of the reaction solution obtained from the above reaction for 1 minute, 2 minutes, 3 minutes, 4 minutes, and 5 minutes using a UV-2600 ultraviolet spectrophotometer from Shimadzu Corporation of Japan. The absorption peaks produced by silver nanoparticles are all around 435nm, which produces obvious plasmon resonance ...
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