Sealant for battery component, battery component and sealing method thereof
A technology for battery components and sealants, applied in battery pack parts, sealing materials, electrical components, etc., can solve the problems of unmentioned oxygen permeability of sealants, bonding strength to be improved, and failure to know solar cells. , to achieve long-term stable adhesion, low water vapor permeability and oxygen permeability, and maintain the effect of adhesion
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Synthetic example 1
[0135] Synthesis Example 1 Linear organopolysiloxane (A-1) of the present invention
[0136] In a 4L four-necked flask equipped with a stirrer, a thermometer, a condenser and a dropping funnel, add 130.08g (0.50mol) of 1,4-bis(dimethylmethoxysilyl)cyclohexane and 60.03g ( 0.50mol) of dimethyldimethoxysilane, and the temperature was raised to 50°C. Under stirring conditions, slowly dropwise add a mixed solution containing 1100g deionized water and 15g hydrochloric acid (concentration: 5N) into the flask, then slowly add 8.51g (0.05mol) cyclohexenyl dimethyl methoxy base silane. After the dropwise addition, the inner temperature of the flask was maintained at 50° C., and the reaction was continued for 4 hours under stirring. The reaction product was left standing to separate the layers, the water phase was separated, and the collected organic phase was washed with water until neutral. Sodium sulfate was added to the organic phase washed with water for drying, and the sodium...
Synthetic example 2
[0138] Synthesis Example 2 Straight-chain organohydrogenpolysiloxane (B-1) according to the present invention
[0139] Place a 4L four-necked flask equipped with a stirrer, a thermometer, a condenser and a dropping funnel in an ice bath, and add 104.06g (0.40mol) of 1,4-bis(dimethylmethoxysilyl) to the flask Cyclohexane and 31.82 g (0.30 mol) methyldimethoxysilane. Under stirring conditions, a mixed solution containing 800 g of deionized water and 12 g of hydrochloric acid was slowly added dropwise into the flask, and then 5.20 g (0.05 mol) of trimethylmethoxysilane was slowly added dropwise into the flask. After the dropwise addition, the inner temperature of the flask was maintained below 5°C, and the reaction was continued for 4 hours under stirring conditions. The reaction product was left standing to separate the layers, the water phase was separated, and the collected organic phase was washed with water until neutral. Sodium sulfate was added to the organic phase was...
Synthetic example 3
[0141] Synthesis Example 3 Branched-chain organohydrogenpolysiloxane (C-1) of the present invention
[0142] Place a 4L four-neck flask equipped with a stirrer, thermometer, condenser and dropping funnel in an ice bath, and add 116.86g (292.15 0.40mol) of 1,4-bis(methyldimethoxysilyl) to the flask ) cyclohexane and 14.75 g (134.060.11 mol) tetramethyldisiloxane. Under the condition of stirring, slowly dropwise add the mixed solution containing 500g deionized water and 6g hydrochloric acid (concentration is 5N) in the flask. After the dropwise addition, the inner temperature of the flask was maintained below 5°C, and the reaction was continued for 4 hours under stirring conditions. The reaction product was left standing to separate the layers, the water phase was separated, and the collected organic phase was washed with water until neutral. Sodium sulfate was added to the organic phase washed with water for drying, and the sodium sulfate was filtered off after drying. The...
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Abstract
Description
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Application Information
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