A nanopowder with dual detection effects on temperature and pH and its preparation method
A nano-powder, dual technology, applied in thermometers, chemical instruments and methods, thermometers with physical/chemical changes, etc., can solve problems such as limited, achieve high sensitivity, simple method, small size effect
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Embodiment 1
[0033] A method for preparing a nanopowder with dual detection effects on temperature and pH, the preparation method comprising the following processes:
[0034] (1) First, put silk fibroin powder, sodium phosphate, and biphenyl dicarboxylic acid in deionized water, stir for 30 minutes, then centrifuge the powder from the mixed solution, roll it once, and first place it at 70-90°C Pre-bake for 5 minutes, then bake at a high temperature of 150-160°C for 3 minutes, rinse with deionized water for 5 times, and dry to obtain the first aromatic polycarboxylic acid modified powder; powder, sodium phosphate, biphenyl dicarboxylate The mass ratio is 1:5:8
[0035] (2) Place the powder, catalyst, and aromatic polycarboxylic acid modified by aromatic polycarboxylic acid for the first time in deionized water, repeat the operation of step (1), the number of repetitions is 3 times, and obtain multiple aromatic polycarboxylic acid Modified powder;
[0036] (3) Powder modified with multiple...
Embodiment 2
[0038] A method for preparing a nanopowder with dual detection effects on temperature and pH, the preparation method comprising the following processes:
[0039] (1) First, put silk fibroin powder, sodium phosphate, and terephthalic acid in deionized water, stir for 30 minutes, then centrifuge the powder from the mixed solution, roll it once, and pre-heat at 70-90°C. Bake for 5 minutes, then bake at a high temperature of 150-160°C for 3 minutes, rinse with deionized water for 5 times, and dry to obtain the first aromatic polycarboxylic acid modified powder; the quality of the powder, sodium phosphate, and terephthalic acid The ratio is 1:5:8;
[0040] (2) Place the powder, catalyst, and aromatic polycarboxylic acid modified by aromatic polycarboxylic acid for the first time in deionized water, repeat the operation of step (1), and repeat the number of times for 3 times to obtain multiple aromatic polycarboxylic acid Modified powder;
[0041] (3) Powder modified with multiple...
Embodiment 3
[0043]A method for preparing a nanopowder with dual detection effects on temperature and pH, the preparation method comprising the following processes:
[0044] (1) First, put silk fibroin powder, sodium phosphate, biphenyl dicarboxylic acid and 4-hydroxypyridine-2,6-dicarboxylic acid in deionized water, stir for 30 minutes, and then centrifuge the powder from the mixed solution , rolled once, pre-baked at 70-90°C for 5 minutes, then baked at a high temperature of 150-160°C for 3 minutes, rinsed with deionized water for 5 times, and dried to obtain the first aromatic polycarboxylic acid modified powder body; the mass ratio of biphenyl dicarboxylic acid to 4-hydroxypyridine-2,6-dicarboxylic acid is 1:1, and the mass ratio of powder, sodium phosphate, and hydroxycarboxylic acid is 1:5:8;
[0045] (2) Place the powder, catalyst, and aromatic polycarboxylic acid modified by aromatic polycarboxylic acid for the first time in deionized water, repeat the operation of step (1), the nu...
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