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Automatic cleaning device for glass sample bottles

A technology for automatic cleaning and sample bottles, applied in the direction of cleaning hollow objects, cleaning methods and utensils, chemical instruments and methods, etc., can solve the problems of large amount of organic solvent, consumption of organic solvent, low cleaning efficiency, etc., and achieve high degree of automation, Achieve quantitative recovery and high cleaning efficiency

Inactive Publication Date: 2018-05-11
BEIJING RES INST OF URANIUM GEOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The cleaning of a large number of sample bottles requires a lot of energy from the experimenters, and consumes a lot of organic solvents, which is not good for the environment.
At present, there are roughly two ways to clean the sample bottle: one is to soak a large amount of organic solvent in a closed container, and to replace the fresh solvent several times to achieve the purpose of cleaning. This method can achieve the purpose of cleaning the sample bottle, but The amount of organic solvent that needs to be consumed is particularly large, which puts pressure on the treatment of organic waste liquid; the second method is to fumigate with an organic solvent in a closed container, and clean it by condensing the vapor of the organic solvent in the sample bottle. Realize the reuse of organic solvents, but the cleaning efficiency is low and time-consuming

Method used

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  • Automatic cleaning device for glass sample bottles
  • Automatic cleaning device for glass sample bottles
  • Automatic cleaning device for glass sample bottles

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Step 1, connect the devices in order, add chromatographically pure methylene chloride in reagent bottle I, and add chromatographically pure n-hexane in reagent bottle II;

[0037] Step 2. Turn on the power, select the plunger pump made of PEEK, and set the cleaning event as follows: from 0 to 6 minutes, run pump A, set the flow rate of dichloromethane to 2.5ml / min; from 6 to 12 minutes, run pump B, set The flow rate of n-hexane is 2.5ml / min, and the total running time is 12min;

[0038] Step 3: Select a roulette with 60 positions and 1.5ml sample bottles, place the sample bottles upside down in the fixed slots respectively; use double nozzles for cleaning.

[0039] Step 4. Close the glass cover to ensure the seal;

[0040] Step 5. Connect the waste liquid collection bottle;

[0041] Step 6. Turn on the speed regulating motor and set the speed to 1r min -1 ;

[0042] Step 7. Start the plunger pump and start cleaning;

[0043] Step 8: After cleaning, take out the sam...

Embodiment 2

[0045] Step 1. Connect the devices in sequence, add chromatographically pure methanol to reagent bottle I, and add chromatographically pure n-hexane to reagent bottle II;

[0046] Step 2. Turn on the power, select a stainless steel plug pump, and set the cleaning event as follows: from 0 to 10 minutes, run pump B, set the flow rate of n-hexane to 5ml / min; from 10 to 15 minutes, run pump A, set the flow rate of methanol to 2.5ml / min, the total running time is 15min;

[0047] Step 3: Select a roulette with 120 positions and 1.5ml sample bottles, place the sample bottles upside down in the fixed slots respectively; use three nozzles for cleaning.

[0048] Step 4. Close the glass cover to ensure the seal;

[0049] Step 5. Connect the waste liquid collection bottle;

[0050] Step 6. Turn on the speed regulating motor and set the speed to 10r min -1 ;

[0051] Step 7. Start the plunger pump and start cleaning;

[0052] Step 8: After cleaning, take out the sample bottle.

Embodiment 3

[0054] Step 1, connect the devices in order, add chromatographically pure methanol in reagent bottle I, and add chromatographically pure methylene chloride in reagent bottle II;

[0055] Step 2. Turn on the power, select a stainless steel plug pump, and set the cleaning event as follows: from 0 to 10 minutes, run pump B and set the flow rate of methylene chloride to 5ml / min; from 10 to 15 minutes, set the flow rate of pump A to 2.5ml / min. min, the flow rate of pump B is 2.5ml / min; from 15 to 20min, run pump A, set the flow rate of methanol to 5ml / min; the total running time is 20min;

[0056] Step 3: Select a roulette with 30 positions and 5ml sample bottles, place the sample bottles upside down in the fixed slot; use a single nozzle for cleaning.

[0057] Step 4. Close the glass cover to ensure the seal;

[0058] Step 5. Connect the waste liquid collection bottle;

[0059] Step 6. Turn on the speed regulating motor and set the speed to 5r min -1 ;

[0060] Step 7. Start t...

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PUM

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Abstract

The invention belongs to the technical field of laboratory equipment cleaning and particularly relates to a device capable of cleaning sample introduction bottles automatically. The automatic cleaningdevice for the glass sample bottles aims at overcoming defects of the prior art and achieving the effects that interactive cleaning is conducted in a manner that different types of solvent can be adopted based on different pollutants in the sample bottles, and the automatic cleaning device is high in efficiency and portable. According to the technical scheme, the automatic cleaning device for theglass sample bottles comprises solvent bottles, plunger pumps, a pipeline, support feet, solvent spray heads, the sample bottles, a sample bottle wheel disc, a seal shaft, a speed reduction motor, abase plate, a glass housing, a nozzle base and a seal plug; the base plate is a disc, wherein a through hole is formed in the center of the disc; the glass housing is buckled onto the base plate; theseal plug is arranged between the lower edge of the glass housing and the base plate; the speed reduction motor is arranged below the base plate; the seal shaft is arranged on the speed reduction motor, penetrates the central through hole of the base plate and extends into the glass housing; and the sampled bottle wheel disc is arranged at the upper end, inside the glass housing, of the seal shaft.

Description

technical field [0001] The invention belongs to the technical field of laboratory equipment cleaning, in particular to an automatic cleaning device for glass sample bottles. Background technique [0002] A large number of glass sample vials are used in the analysis and testing of organic matter. As the requirements for analysis and testing become higher and higher, the cleanliness of the sample vials is also getting higher and higher. Both newly purchased vials and used vials require cleaning. The cleaning of a large number of sample vials requires a lot of energy of the experimenters and consumes a lot of organic solvents, which is not good for the environment. At present, there are roughly two ways to clean the sample bottle: one is to soak a large amount of organic solvent in a closed container, and to replace the fresh solvent several times to achieve the purpose of cleaning. This method can achieve the purpose of cleaning the sample bottle, but The amount of organic s...

Claims

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Application Information

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IPC IPC(8): B08B9/32B08B9/28
CPCB08B9/28B08B9/32
Inventor 李伯平范增伟刘桂方崔建勇郭冬发
Owner BEIJING RES INST OF URANIUM GEOLOGY
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