A kind of water-based heat-activated adhesive for oil filter and preparation method thereof
A technology of oil filter and heat activation, which is applied in the direction of adhesives, rosin adhesives, polymer adhesive additives, etc., can solve the problems of poor initial adhesion and adhesive layer back-adhesion, etc., and achieve enhanced bonding strength and improved Excellent water resistance and compatibility
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Embodiment 1
[0031] The preparation of embodiment 1 modified rosin resin
[0032] Get 100g of hydrogenated rosin and dissolve in ethanol to make a solution with a concentration of 10% (m / v), then add 0.03g of 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, Mix evenly, slowly add 50g of diglycolamine dropwise under stirring condition, react at room temperature for 60min, then raise the temperature to 80°C, slowly volatilize and remove ethanol until the drying is completed, and the product is obtained.
Embodiment 2
[0033] Preparation of embodiment 2 modified rosin resin
[0034] Get 100g of hydrogenated rosin and dissolve in ethanol to make a solution with a concentration of 10% (m / v), then add 0.05g of 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, Mix evenly, slowly add 60g of diglycolamine dropwise under stirring condition, react at room temperature for 60min, then raise the temperature to 80°C, slowly volatilize and remove ethanol until the drying is complete, and the product is obtained.
Embodiment 3-4
[0035] Preparation of embodiment 3-4 and comparative example 1-5 water-based heat-activated adhesive
[0036] Embodiment 3-4 and comparative example 1-5 water-based heat-activated adhesive comprise components and parts by weight thereof shown in the table below:
[0037]
[0038]
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