Method for rapidly measuring content of cellulose in sargassum horneri with near-infrared spectroscopy technology

A near-infrared spectroscopy and cellulose content technology is applied in the field of rapid determination of cellulose content of copper algae, which can solve the problems of cumbersome determination steps, huge error in the determination result of seaweed cellulose content, and high cost, and achieves the effect of improving the quality control level.

Inactive Publication Date: 2018-06-19
ZHEJIANG UNIV OF TECH
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Problems solved by technology

If the above-mentioned national standard is used to measure the cellulose content, not only the measurement takes up to 2 to 3 days, but also because the measurement object of the national standard method embodiment is ramie and wood, it is not necessarily applicable to the determination of seaweed cellulose. In the actual measurement process It is also found that the measurement results of seaweed cellulose content obtained by this method have a large error
Other available methods include Van Soest and its improved method and chromatographic method, wherein, Van Soest and its improved method can simultaneously measure the contents of cellulose content, moisture, hemicellulose, lignin and ash, but the determination steps are cumbersome and time-consuming. If gas chromatography, high performance liquid chromatography and other chromatographic methods are used, although the measurement results are relatively accurate, there are disadvantages of high cost and long time consumption
[0005] It can be seen that the traditional methods for quantitative analysis of cellulose content in seaweed generally have the disadvantages of cumbersome determination steps and long time consumption, and the chromatography method has the disadvantage of high testing cost, which limits the promotion and application of these methods in the actual production process

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  • Method for rapidly measuring content of cellulose in sargassum horneri with near-infrared spectroscopy technology
  • Method for rapidly measuring content of cellulose in sargassum horneri with near-infrared spectroscopy technology
  • Method for rapidly measuring content of cellulose in sargassum horneri with near-infrared spectroscopy technology

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Embodiment Construction

[0036] The implementation of the present invention will be described in detail below with reference to the accompanying drawings and preferred embodiments.

[0037] refer to Figure 1 to Figure 5 , a kind of method utilizing near-infrared spectroscopic technology to measure the cellulose content of copper algae rapidly, comprises the following steps:

[0038] The first step is to collect samples of copper algae from different sources or batches, and perform necessary sample pretreatment.

[0039] The copper algae samples collected in the preferred embodiment of the present invention come from the Wenzhou sea area in southern Zhejiang, and a total of 40 copper algae samples were collected. After the sample was washed with water to remove the attached sediment and salt, it was placed in the sun to dry briefly, and then dried at 105°C. The washed and dried copper algae sample was crushed with a pulverizer and passed through a multi-layer sieve. , Take a 60 mesh sample and put i...

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Abstract

A method for rapidly measuring content of cellulose in sargassum horneri with a near-infrared spectroscopy technology comprises steps as follows: S1, acquisition and pretreatment of a sargassum horneri sample; S2, measurement of the content of cellulose in the sargassum horneri sample with an improved sulfuric acid and potassium dichromate oxidation method; S3, acquisition of near-infrared spectrum of the sargassum horneri sample through scanning by a near-infrared spectrometer; S4, establishment and evaluation of a near-infrared spectrum quantitative analysis model; S5, application of the near-infrared spectrum quantitative analysis model. The method has the advantages of being rapid, accurate and environmentally friendly, is favorable for improving the quality control level of the content of the cellulose in sargassum horneri and can be popularized and applied to quality control of other seaweed biomass.

Description

technical field [0001] The invention belongs to the field of cellulose content analysis, and in particular relates to a method for rapidly determining the cellulose content of copper algae based on near-infrared spectroscopy. Background technique [0002] Marine biomass resources represented by macroalgae have the advantage of not occupying land and freshwater resources, and have great development potential. Copper algae (Sargassum horneri (Turn.) Ag. commonly known as "Lilac House", belonging to the genus Sargassum (Sargassum), distributed in the coastal shallow sea area of ​​China), hijiki and asparagus and other large seaweed plants are tall, with luxuriant branches and leaves. Known as the "sea forest", it is an ideal place for marine organisms to avoid enemies, feed, and lay eggs, and it is easy to scale artificial cultivation and environmental restoration (absorb nitrogen, phosphorus and heavy metals in the environment, release oxygen, adjust the pH of the water body, ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/359
CPCG01N21/359
Inventor 艾宁蒋益波夏陆岳王祁宁应惠娟
Owner ZHEJIANG UNIV OF TECH
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