Pharmaceutical composition for preventing and treating femoral head necrosis and preparation method thereof
A technology of femoral head necrosis and composition, which is applied in the field of pharmaceutical composition for preventing and treating femoral head necrosis and its preparation, which can solve the problems of low active ingredient content, rough preparation process, and complicated medicinal ingredients, and achieve short treatment cycle and effective treatment of femoral head. Bone necrosis, the effect of reducing the risk of contamination
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Embodiment 1
[0041] Embodiment 1 Bozi kernel pretreatment
[0042] (1) After mixing the cypress kernels and the porous starch in a weight ratio of 1:0.4, place them in a pressure alternation generator, and continuously feed the mixed liquid steam. The mixed liquid contains 75% v / v of absolute ethanol, Water 10% v / v, phytic acid ester 15% v / v, and the ratio of the mixed liquid to the cypress kernel is 1g / 40mL, then apply an alternating pressure of 0-15MP, treat for 25min, the pressure The increasing or decreasing frequency is 3MP / 5min, and then dried at a low temperature of 50°C to obtain material A, which is set aside;
[0043] (2) Put the material A treated in step (1) under an ultraviolet lamp for irradiating treatment for 30 minutes, then wash with alcohol and water in sequence, repeat this 4 times, and dry at a low temperature at 50°C to obtain Baiziren .
Embodiment 2
[0052] Example 2 Evaluation of the Degradation Effect of Aflatoxin in Baiziren
[0053] The aflatoxin and fat content of the Baizi kernels treated by the methods of Example 1 and Comparative Examples 1 and 2 were tested respectively, and the results are shown in Table 1 below.
[0054] Table 1 The effect of pretreatment on the degradation of aflatoxin and fat level in Baiziren
[0055]
[0056] It can be seen from Example 1 that the pretreatment step of the cypress kernels provided by the present invention can effectively degrade aflatoxins B1 and B2, so that the treated cypress kernels are almost free of aflatoxins B1 and B2, and the degradation rate reaches more than 99.69%. And it has little effect on the fat level of Baiziren, and does not affect the nutrients of Baiziren.
Embodiment 3
[0057] Embodiment 3 is used for preventing and treating the preparation of the pharmaceutical composition of femoral head necrosis
[0058] Formula: 400 parts of rehmannia glutinosa, 450 parts of yam, 450 parts of Baiziren, 300 parts of tortoise shell, 250 parts of Polygonum multiflorum and 150 parts of angelica.
[0059] Preparation:
[0060] (1) Take by weighing the Chinese yam of prescription 1 / 3 amount, be ground into fine powder, set aside;
[0061] (2) Mix the remaining 2 / 3 of yam with Rehmannia glutinosa, Boziren, Guijia, Radix Polygoni Multiflori and Angelica, then put it in a multi-functional extraction tank and add water to decoct twice, adding 6 times the amount of water for the first time , for the second time, add 5 times the amount of water of the medicinal materials, decoct for 2 hours each time, and collect volatile oil at the same time;
[0062] (3) Filter the two decoctions, combine the decoctions, concentrate the filtrate to a relative density of 1.10 at 7...
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