A kind of preparation method of concrete curing agent
A concrete curing agent and catalyst technology, applied in the field of curing agents, can solve the problems of easy efflorescence and poor durability, and achieve the effects of avoiding efflorescence, increasing permeability, and accelerating curing rate.
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[0019] A preparation method of a concrete curing agent. The preparation method includes the following steps:
[0020] (1) According to the mass ratio of 6:1:12~16, take tetrabutyl titanate, aminophenyltrialkoxysilane and anhydrous ethanol for 15min ultrasonic vibration, and then add 3~5 times the mass of anhydrous ethanol 0.01 mol / L citric acid solution, mix evenly, put it into the reaction kettle, add 5-10% of the weight of tetrabutyl titanate additives, stir at 60-80℃ for 2h;
[0021] (2) After the stirring, cool to room temperature and discharge, collect the discharged material, sonicate and centrifuge the discharged material, collect the precipitate, dry the precipitate at 90°C, crush, pass through a 500 mesh sieve, and collect Sieving the particles, ball milling the sieved particles and nano-silica at a mass ratio of 3-6:5 at 800r / min for 40 minutes, and collect the ball-milled material;
[0022] (3) In parts by weight, take 50-60 parts of acetone, 30-35 parts of toluene, 20-25...
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