Preparation method of flame-retardant stable polyurethane reinforcing material
A reinforcement material, polyurethane technology, applied in the field of reinforcement materials, can solve problems such as poor flame retardancy and poor mechanical properties, and achieve the effects of improving mechanical properties, improving dispersion, and expanding the scope of application
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[0017] According to the mass ratio of 1:15, stir and mix peat and 1mol / L sodium hydroxide solution and place it in a mortar for grinding and dispersing for 2-3 hours to obtain a grinding slurry and place it under 200-300W for ultrasonic dispersion for 10-15 minutes to obtain a dispersion Place it in a water bath at 75-80°C for 3-5 hours, let it cool down to room temperature, then centrifuge at 2500-3000r / min for 10-15 minutes, collect the supernatant, add glacial acetic acid dropwise to adjust the pH to 2.5, and let it stand After 6-8 hours, vacuum freeze-dry and collect the dry particles, modified particles; weigh 45-50 parts of Baume degree 15 silica sol, 25-30 parts of deionized water, 10-15 parts of modified The granules and 25-30 parts by mass fraction of 25% ethanol solution are placed in a three-necked flask, then heated in a water bath at 65-75°C for 20-24 hours, and left to cool to room temperature to obtain a gel solution; in parts by weight, respectively Weigh 25 to...
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