High-acid-solubility plugging liquid during drilling
A plugging while drilling and high-acid technology, which is applied in the field of oil well plugging, can solve the problems of excessive mineral particle density, high density and brittleness of mica sheets, and easy floating of mixed slurry, and achieve strong pressure bearing capacity, excellent hardness and flexibility , Improve the effect of the ability to support pores and cracks
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Embodiment 1
[0050] 1. Raw material preparation
[0051] (1) Drilling mud
[0052] Select the drilling mud used in the oil field.
[0053] (2) Aluminum alloy particles GYD
[0054] The density of aluminum alloy particles GYD is 2.3-2.6g / cm 3 , the fineness is 6.7-0.17mm.
[0055] (3) Superfine calcium
[0056] Use superfine calcium carbonate powder with a fineness of 300-600 mesh.
[0057] (4) Flexible polymer materials
[0058] (i) Preparation of (meth)acrylate rubber
[0059] (a) 50g n-butyl methacrylate and 8g tetrafluoroethylene are mixed homogeneously;
[0060](b) 1g benzoyl peroxide is added in 100g dimethylbenzene, and stir;
[0061] (c) adding the xylene solution in step (ii) to the monomer mixture in step (i), initiating a polymerization reaction at 60-90° C. to obtain (meth)acrylate rubber.
[0062] (ii) Preparation of flexible polymer materials
[0063] (a) adding 50 g of waste tire rubber powder and 50 g of (meth)acrylate rubber prepared in step (1) into a high-speed ...
Embodiment 2
[0072] 1. Raw material preparation
[0073] (1) Drilling mud
[0074] Select the drilling mud used in the oil field.
[0075] (2) Aluminum alloy particles GYD
[0076] The density of aluminum alloy particles GYD is 2.3-2.6g / cm3, and the fineness is 6.7-0.17mm.
[0077] (3) Superfine calcium
[0078] Use superfine calcium carbonate powder with a fineness of 300-600 mesh.
[0079] (4) Flexible polymer materials
[0080] (i) Preparation of (meth)acrylate rubber
[0081] (a) 60g of 2-ethylhexyl acrylate and 12g of ethylene difluoride are mixed uniformly;
[0082] (b) 1g benzoyl peroxide is added in 100g cyclohexanone, and stir;
[0083] (c) adding the xylene solution in step (ii) to the monomer mixture in step (i), initiating a polymerization reaction at 60-90° C. to obtain (meth)acrylate rubber.
[0084] (ii) Preparation of flexible polymer materials
[0085] (a) Add 45g of waste tire rubber powder and 55g of (meth)acrylate rubber prepared in step (1) into a high-speed o...
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