Anti-corrosion environment barrier coating, preparation method and application of anti-corrosion environment barrier coating and engine
An environmental barrier and corrosion-resistant technology, applied in the field of materials, can solve problems such as lack of better, achieve the effects of short time consumption, extended reliability and overall service life, and simple preparation methods
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[0028] The preparation method of the corrosion-resistant environment barrier coating provided by the embodiment of the present invention includes the following steps: using a plasma spraying-physical vapor deposition method, preparing an Si coating on the surface of the substrate in sequence, and preparing a Si coating on the surface of the Si coating on the side away from the substrate. Prepare a mullite coating and prepare Yb on the surface of the side of the mullite coating away from the Si coating 2 SiO 5 Coating, environmental barrier coating. An aluminum film layer is prepared on the surface of the environmental barrier coating to obtain an aluminum-plated sample. Vacuum heat treatment of aluminum-plated samples to obtain a corrosion-resistant environment barrier coating.
[0029]Optionally, the raw material of the matrix includes a silicon carbide-based composite material, and the silicon carbide-based composite material includes a SiC / SiC composite material. Among t...
Embodiment 1
[0061] Using the SiC / SiC composite material as the matrix, use gasoline, acetone and alcohol to decontaminate and clean the matrix in sequence for 10 minutes, then install the matrix on the fixture and place it in a vacuum tank, evacuate the vacuum tank to 0.45mbar, and then backfill it with argon Gas to 38mbar, and then vacuum to 1.45mbar.
[0062] A Si coating with a thickness of 45 μm and Si powder with a particle size of 15 μm as raw material was prepared on the surface of the cleaned substrate by plasma spraying-physical vapor deposition technology. The plasma spraying conditions in the Si coating preparation process are as follows: the net power of plasma spraying is 40kW, the flow rate of argon gas in the plasma gas is 90NSPM, the flow rate of hydrogen gas is 5NSPM, the powder feeding rate is 15g / min, the spraying distance is 300mm, and the temperature of the substrate is 890°C.
[0063] A mullite coating with a thickness of 45 μm and agglomerated mullite powder with a...
Embodiment 2
[0069] Using the SiC / SiC composite material as the substrate, use gasoline, acetone and alcohol to decontaminate and clean the substrate by ultrasonic for 15 minutes, then install the substrate on the fixture and place it in a vacuum tank, evacuate the vacuum tank to 0.55mbar, and then backfill it with argon Gas to 42mbar, and then vacuum to 1.55mbar.
[0070] A Si coating with a thickness of 55 μm and Si powder with a particle size of 45 μm as raw material was prepared on the surface of the cleaned substrate by plasma spraying-physical vapor deposition technology. The plasma spraying conditions in the Si coating preparation process are as follows: the net power of plasma spraying is 50kW, the flow rate of argon gas in the plasma gas is 120NSPM, the flow rate of hydrogen gas is 10NSPM, the powder feeding rate is 20g / min, the spraying distance is 500mm, and the temperature of the substrate is 910°C.
[0071] A mullite coating with a thickness of 55 μm and agglomerated mullite ...
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