Rapid baking type tundish dry material and preparation method thereof
A rapid and raw material technology, applied in the field of refractory materials, can solve the problems that the baking effect cannot meet the use requirements, affect the service life of refractory materials, poor compactness and bonding strength, etc., achieve good application prospects, improve thermal conductivity and cost low effect
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Embodiment 1
[0024] The raw material components of the fast-baking tundish dry material are 66% by weight of sintered magnesia particles, 17% of sintered magnesia fine powder, 10% of metal iron powder, 5% of carbonaceous binder, and 2% of additives. %; Described carbonaceous binding agent is phenolic resin, and the weight content of its fixed carbon is 46.2%; Described additive is alumina powder, and its Al 2 o 3 The weight content is 98.5%, the particle size is ≤325 mesh;
[0025] Among them, the sintered magnesia particles are the part of the sintered magnesia with a particle size of ≤3mm and >200 mesh, and the sintered magnesia fine powder is the part of the sintered magnesia with a particle size of ≤200 mesh; the weight percentage of the sintered magnesia particles and the sintered magnesia fine powder ≥90%; Fe weight percentage in metal iron powder ≥95%, particle size ≤180 mesh;
[0026] The preparation method is:
[0027] Premix sintered magnesia fine powder, metallic iron powder,...
Embodiment 2
[0032] The raw material components of the fast-baking tundish dry material are 64% by weight of sintered magnesia particles, 24% of sintered magnesia fine powder, 5% of metal iron powder, 4% of carbonaceous binder, and 3% of additives. %; the carbonaceous binder is industrial sucrose; the additive is silicon powder, with a weight purity ≥ 98%, and a particle size ≤ 200 mesh; all the other are the same as in Example 1;
[0033] Method is with embodiment 1, and difference is:
[0034] The premixing time is 23 minutes, and the sintered magnesia particles are added and mixed for 20 minutes;
[0035] After the dry material of the tundish is formed by vibration construction, it is baked at 1000°C for 1.0h to make a tundish working lining with a thickness of 100mm, and its bulk density is 2.72g / cm 3 , the apparent porosity is 21.5%, and the normal temperature compressive strength is 42.3MPa; the service life of the working lining of the tundish is 28 hours.
Embodiment 3
[0037] The raw material components of the fast-baking tundish dry material are 65% by weight of sintered magnesia particles, 20% of sintered magnesia fine powder, 8% of metal iron powder, 4.5% of carbonaceous binder, and 2.5% of additives. %; Described carbonaceous binding agent is the equal mass mixture of phenolic resin and industrial sucrose; Described additive is B 4 C powder, weight purity ≥ 98%, particle size ≤ 200 orders; all the other are the same as embodiment 1;
[0038] Method is with embodiment 1, and difference is:
[0039] The premixing time is 25 minutes, and the sintered magnesia particles are added and mixed for 18 minutes;
[0040] After the dry material of the tundish is formed by vibration construction, it is baked at 950°C for 1.5h to make a tundish working lining with a thickness of 80mm, and its bulk density is 2.76g / cm 3 , the apparent porosity is 20.8%, and the normal temperature compressive strength is 35.2MPa; the service life of the working lining...
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Abstract
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