Rapid baking type tundish dry material and preparation method thereof
A rapid and raw material technology, applied in the field of refractory materials, can solve the problems that the baking effect cannot meet the use requirements, affect the service life of refractory materials, poor compactness and bonding strength, etc., achieve good application prospects, improve thermal conductivity and cost low effect
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[0023] Example 1
[0024] The raw material components of the quick-baking tundish dry material account for 66% by weight of sintered magnesia particles, 17% of sintered magnesia fine powder, 10% of metal iron powder, 5% of carbonaceous binder, and 2% of additives. %; the carbonaceous binder is phenolic resin, and the weight content of its fixed carbon is 46.2%; the additive is alumina powder, and its Al 2 O 3 The weight content is 98.5%, and the particle size is less than or equal to 325 meshes;
[0025] Among them, the sintered magnesia particles are the part of the sintered magnesia with a particle size of ≤3mm and >200 mesh, and the sintered magnesia fine powder is the part of the sintered magnesia with a particle size of ≤200 mesh; the weight percentage of MgO in the sintered magnesia particles and the sintered magnesia fine powder ≥90%; Fe weight percentage in metal iron powder ≥95%, particle size ≤180 mesh;
[0026] The preparation method is:
[0027] Premix sintered...
Example Embodiment
[0031] Example 2
[0032] The raw material components of the quick-baking tundish dry material account for 64% of sintered magnesia particles, 24% of sintered magnesia fine powder, 5% of metal iron powder, 4% of carbonaceous binder, and 3% of additives. %; the carbonaceous binder is industrial sucrose; the additive is silicon powder, the weight purity is ≥98%, and the particle size is ≤200 mesh; the rest are the same as in Example 1;
[0033] The method is the same as in Example 1, except that:
[0034] The pre-mixing time is 23 minutes, and the sintered magnesia particles are added and mixed for 20 minutes;
[0035] After the tundish dry material is formed by vibration construction, it is baked at 1000℃ for 1.0h to make a tundish working lining with a thickness of 100mm, and its bulk density is 2.72g / cm 3 , the apparent porosity is 21.5%, the compressive strength at room temperature is 42.3MPa; the service life of the tundish working lining is 28 hours.
Example Embodiment
[0036] Example 3
[0037] The raw material components of the quick-baking tundish dry material account for 65% by weight of sintered magnesia particles, 20% of sintered magnesia fine powder, 8% of metal iron powder, 4.5% of carbonaceous binder, and 2.5% of additives. %; the carbonaceous binder is an equal quality mixture of phenolic resin and industrial sucrose; the additive is B 4 C powder, weight purity ≥98%, particle size ≤200 mesh; the rest are the same as in Example 1;
[0038] The method is the same as in Example 1, except that:
[0039] The pre-mixing time is 25 minutes, and the sintered magnesia particles are added and mixed for 18 minutes;
[0040] After the tundish dry material is formed by vibration construction, it is baked at 950℃ for 1.5h to make a tundish working lining with a thickness of 80mm, and its bulk density is 2.76g / cm 3 , the apparent porosity is 20.8%, the compressive strength at room temperature is 35.2MPa; the service life of the tundish working ...
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