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Carbon black modifying technology and device

A carbon black and modification technology, applied in the direction of fibrous fillers, etc., can solve the problems of easy introduction of other by-products and impurities, low stability of dispersion system, unfavorable industrial production, etc., achieve simple oxidation treatment process and improve dispersion performance Its stability and the effect of easy industrial production

Inactive Publication Date: 2018-10-12
四川迈克兰诺气泡科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The invention provides a carbon black modification process, which is used to solve the problem that the traditional carbon black modification process has low dispersion system stability, easy introduction of other by-products and impurities, long modification process route, cumbersome operation, and is not conducive to industrial production. technical problems; and design a carbon black improvement device for the carbon black modification process to provide guarantee for the realization of the carbon black modification process

Method used

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  • Carbon black modifying technology and device
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  • Carbon black modifying technology and device

Examples

Experimental program
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Effect test

Embodiment 1

[0029] A carbon black modification process, which is a process of dispersing and grinding carbon black powder into a carbon black slurry, and injecting ozone micro-nano bubbles into the carbon black slurry to oxidize the carbon black and enhance the water-based The method of dispersion stability in the system; the method specifically includes the following steps:

[0030] (1) Add 5Kg of carbon black and 20Kg of deionized water to the carbon black modification device, disperse and grind at a speed of 3m / s for 1 to 1.5 hours, make the carbon black and deionized water fully contact and wet, and open the secondary agglomeration Pellets to obtain charcoal black paste;

[0031] (2) The ozone with a mass percentage concentration of 3% and a flow rate of 2.5L / min is passed through the micro-nano bubble generator to form bubbles into the carbon black slurry, and the speed of the carbon black modification device is increased to 5m / s. , Continue to disperse and grind for 8-12 hours, until th...

Embodiment 2

[0034] A carbon black modification process. The process is to disperse and grind carbon black powder into a carbon black slurry, and pass ozone micro-nano bubbles into the carbon black slurry to oxidize the carbon black and enhance the carbon black A method of dispersion stability in an aqueous system; the method specifically includes the following steps:

[0035] (1) Same as Example 1;

[0036] (2) The ozone with a mass percentage concentration of 3% and a flow rate of 2.5L / min is passed through the micro-nano bubble generator to form bubbles into the carbon black slurry, and the speed of the carbon black modification device is increased to 5m / s. , Continue to disperse and grind for 8-12 hours, until the PH value of the carbon black slurry decreases to 3.2-3.4, the oxidation modification of the carbon black is completed, and the modified carbon black slurry is obtained; among them, the micro-nano bubble generator is porous ceramic Plate, the diameter of the ozone micro-nano bubbl...

Embodiment 3

[0039] A carbon black modification process. The process is to disperse and grind carbon black powder into a carbon black slurry, and pass ozone micro-nano bubbles into the carbon black slurry to oxidize the carbon black and enhance the carbon black A method of dispersion stability in an aqueous system; the method specifically includes the following steps:

[0040] (1) Same as Example 1;

[0041] (2) The ozone with a mass percentage concentration of 3% and a flow rate of 2.5L / min is passed through the micro-nano bubble generator to form bubbles into the carbon black slurry, and the speed of the carbon black modification device is increased to 5m / s. , Continue to disperse and grind for 8-12 hours, until the PH value of the carbon black slurry decreases to 3.2-3.4, the oxidation modification of the carbon black is completed, and the modified carbon black slurry is obtained; among them, the micro-nano bubble generator is porous ceramic Plate, the diameter of the ozone micro-nano bubbl...

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Abstract

The invention discloses a carbon black modifying technology. The carbon black modifying technology adopts a method with the following steps of dispersing and grinding the carbon black powder into a carbon black color paste; leading ozone micro-nanometer air bubbles into the carbon black color paste, so as to oxidize and modify the carbon black, and enhance the dispersing stability of the carbon black in a water system. A carbon black modifying device is designed for the carbon black modifying technology, and is used for dispersing and grinding the carbon black color paste, and providing the ozone micro-nanometer air bubbles for the carbon black color paste, so as to provide support for the realization of the carbon black modifying technology. The carbon black modifying technology can solvethe technical problems of the traditional carbon black modifying technology that the stability of the dispersing system is low, other byproducts and impurities are easy to entrap, the modifying technology route is longer, the operation is complicated, and the traditional carbon black modifying technology is not suitable for industrialized production.

Description

Technical field [0001] The invention relates to the technical field of carbon black modification, in particular to a carbon black modification process and device. Background technique [0002] Due to the small particles, large specific surface area, and high surface free energy of carbon black, it is easy to form strong agglomeration forces between carbon black ions, making it hydrophobic and difficult to disperse in aqueous systems. At present, there are a variety of industrial carbon black oxidation modification processes to improve the dispersion performance of carbon black in aqueous systems. For example, various dispersants with many hydrophilic groups and water-absorbing groups are used to modify carbon black; another example is to use nitric acid, hydrogen peroxide, hypochlorite and other oxidants to chemically oxidize carbon black. [0003] Although these methods have more obvious oxidation effects on carbon black, the stability of the dispersion of carbon black in aqueous...

Claims

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Application Information

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IPC IPC(8): C09C1/56
CPCC09C1/565
Inventor 樊载
Owner 四川迈克兰诺气泡科技有限公司
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