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Preparation method of biochar with good electrical property

A technology of electrical properties and bio-carbon, applied in the direction of carbon preparation/purification, etc., can solve problems such as instability and poor electrical properties, and achieve the effects of activating surface properties, enhancing exchange adsorption capacity, and enhancing electrical properties

Active Publication Date: 2018-10-16
安徽省齐岗农业发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, most of the biocarbon materials prepared by the existing technology have problems such as poor electrical properties and instability, and urgently need to be improved.

Method used

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  • Preparation method of biochar with good electrical property

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A method for preparing biochar with good electrical properties, comprising the steps of:

[0037] (1) Cooking treatment:

[0038] Putting the crop stalks into the sodium hydroxide solution and heating to boiling, then boiling for 20 minutes, taking out the crop stalks for later use;

[0039] (2) Oxidation soaking treatment:

[0040] The crop stalks treated in step (1) were soaked in a hydrogen peroxide solution with a volume fraction of 20% for 4 hours, washed with deionized water until neutral and then used for later use;

[0041] (3) Steam explosion treatment:

[0042] Put the crop straw treated in step (2) into a steam explosion tank for steam explosion treatment, take it out after completion, dry and pulverize it, and pass through 100 meshes to obtain crop straw powder for later use;

[0043] (4) Activation treatment:

[0044] Put the crop straw powder obtained in step (3) into the tartaric acid solution for soaking for 5 minutes, take it out, wash it with deion...

Embodiment 2

[0061] A method for preparing biochar with good electrical properties, comprising the steps of:

[0062] (1) Cooking treatment:

[0063] Putting the crop stalks into the sodium hydroxide solution and heating to boiling, then boiling for 25 minutes, taking out the crop stalks for later use;

[0064] (2) Oxidation soaking treatment:

[0065] The crop stalks treated in step (1) were soaked in a hydrogen peroxide solution with a volume fraction of 23% for 5 hours, washed with deionized water until neutral and then used for later use;

[0066] (3) Steam explosion treatment:

[0067] Put the crop straw treated in step (2) into a steam explosion tank for steam explosion treatment, take it out after completion, dry and pulverize it, and pass through 100 meshes to obtain crop straw powder for later use;

[0068] (4) Activation treatment:

[0069] Put the crop straw powder obtained in step (3) into the tartaric acid solution for soaking treatment for 6 minutes, take it out, wash it ...

Embodiment 3

[0086] A method for preparing biochar with good electrical properties, comprising the steps of:

[0087] (1) Cooking treatment:

[0088] Putting the crop stalks into the sodium hydroxide solution and heating to boiling, then boiling for 30 minutes, taking out the crop stalks for later use;

[0089] (2) Oxidation soaking treatment:

[0090] The crop stalks treated in step (1) were soaked in a hydrogen peroxide solution with a volume fraction of 25% for 6 hours, washed with deionized water until neutral and then used for later use;

[0091] (3) Steam explosion treatment:

[0092] Put the crop straw treated in step (2) into a steam explosion tank for steam explosion treatment, take it out after completion, dry and pulverize it, and pass through 100 meshes to obtain crop straw powder for later use;

[0093] (4) Activation treatment:

[0094] Put the crop straw powder obtained in step (3) into the tartaric acid solution for soaking for 7 minutes, take it out, wash it with deion...

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Abstract

The invention discloses a preparation method of a biochar with a good electrical property. The preparation method comprises the following steps: firstly, cooking treatment; secondly, oxidizing immersion treatment; thirdly, steam explosion treatment; fourthly, activation treatment; fifthly, modification treatment; sixthly, carbonization treatment. The preparation method of the biochar, provided bythe invention, has overall process specifications and is convenient for batch operation production; the prepared biochar has excellent electrical properties, so that discharge capacity and cyclic stability are obviously improved and the quality of the biochar serving as a cathode material for a lithium battery is enhanced; the biochar has great market competitiveness and popularization and application value.

Description

technical field [0001] The invention belongs to the technical field of biological carbon processing, and in particular relates to a method for preparing biological carbon with good electrical properties. Background technique [0002] Crop straw is the general term for the stem and leaf parts of mature crops. Usually refers to the remaining parts of wheat, rice, corn, potato, rapeseed, cotton, sugar cane and other crops after harvesting seeds. More than half of the photosynthetic products of crops exist in straw, which is rich in carbon, nitrogen, phosphorus, potassium, calcium, magnesium and organic matter, and is a multi-purpose renewable biological resource. Some of the existing crop stalks are used in the production of biochar. [0003] With the rapid development of social economy, the dependence of human society on energy continues to increase. However, the over-exploitation of human beings has exhausted energy resources and seriously polluted the environment. In ord...

Claims

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Application Information

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IPC IPC(8): C01B32/05
CPCC01B32/05
Inventor 马艳敏
Owner 安徽省齐岗农业发展有限公司