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High-purity hydrogen selenide production equipment and high-purity hydrogen selenide production process based on it

A production equipment and technology of hydrogen selenide, applied in the direction of binary selenium/tellurium compounds, chemical instruments and methods, chemical/physical processes, etc., can solve problems such as inability to remove heavy components, insufficient purity of hydrogen selenide, etc., and achieve energy consumption And the effects of low cost, easy access, and low equipment material requirements

Active Publication Date: 2020-01-10
TAIHE GAS JINGZHOU
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] The present invention will provide a kind of high-purity hydrogen selenide production equipment and the high-purity hydrogen selenide production process based on it, solve the heavy component (such as aromatic solvent, metal impurity etc.) and light component ( Such as nitrogen, hydrogen, methane, carbon dioxide, etc.), resulting in insufficient purity of hydrogen selenide synthesized by the reaction of high-purity hydrogen and selenium particles

Method used

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  • High-purity hydrogen selenide production equipment and high-purity hydrogen selenide production process based on it
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  • High-purity hydrogen selenide production equipment and high-purity hydrogen selenide production process based on it

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Embodiment Construction

[0024] In order to make the technical means, creative features, goals and functions achieved by the present invention clearer and easier to understand, the present invention will be further elaborated below in conjunction with the accompanying drawings and specific embodiments:

[0025] Such as figure 1 , figure 2 ,as well as image 3 Shown, the present invention proposes a kind of high-purity hydrogen selenide production equipment, comprising:

[0026] Reactor 1, which is provided with an inlet for adding selenium particles, catalysts and solvents, the reactor 1 is connected with an inlet pipe 11 for being connected to a hydrogen source, and the reactor 1 includes: a kettle body 12, an agitator 13 and a heater 14 , the heater 14 is connected with the kettle body 12 to heat the material in the reactor 1, the agitator 13 is installed on the kettle body 12, and the stirring blade of the agitator 13 extends into the agitator 13;

[0027] Drier 2, its input end communicates wi...

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Abstract

The invention provides high-purity hydrogen selenide production equipment and a high-purity hydrogen selenide production process based thereon. The high-purity hydrogen selenide production equipment comprises a reaction kettle, a dryer and a heavy-component filter, wherein the reaction kettle is provided with an inlet for feeding selenium particles, a catalyst and a solvent, is communicated with agas feeding pipe for communication to a hydrogen source and comprises a kettle body, a stirrer and a heater; the input end of the dryer is communicated with the top part of the reaction kettle; the input end of the heavy-component filter is communicated with the output end of the dryer, the heavy-component filter comprises a first tank body and a first refrigerator, and the first refrigerator isarranged on the first tank body. The high-purity hydrogen selenide production equipment and the high-purity hydrogen selenide production process provided by the invention have the beneficial effect that the problem of insufficient purity of the hydrogen selenide synthesized by reaction of high-purity hydrogen and the selenium particles due to failure in removing heavy components (such as aromaticsolvents and metal impurities) and light components (such as nitrogen, hydrogen, methane and carbon dioxide) in the prior art is solved.

Description

technical field [0001] The invention relates to the field of hydrogen selenide production, in particular to high-purity hydrogen selenide production equipment and a high-purity hydrogen selenide production process based thereon. Background technique [0002] The Chinese patent discloses a method for preparing and purifying hydrogen selenide with the application number CN200710011160.6, which is that aluminum selenide Al2Se3 reacts with water H2O to generate hydrogen selenide H2Se, and the water in the H2Se gas is removed by condensation; continue to use aluminum selenide After the particles absorb the residual moisture, the H2Se gas enters the steel cylinder to condense and liquefy; the steel cylinder containing the liquid H2Se is evacuated under the cold bath to remove the non-condensable gas impurities dissolved in the liquid; the valve of the steel cylinder is closed to obtain the purified gas directly contained in the steel cylinder Hydrogen selenide: The adsorbent that ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B19/04B01J8/18B01J8/38
CPCB01J8/1827B01J8/382C01B19/04
Inventor 阳辉曾令军何西平汪正宏胡保华
Owner TAIHE GAS JINGZHOU
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