A kind of preparation method of graphene-coated conductive fiber
A conductive fiber and graphene technology, applied in the direction of animal fiber, fiber treatment, fiber type, etc., can solve the problems of poor bonding ability, poor conductivity, and less conductive coating, so as to enhance the conductivity and improve the conductivity. , to avoid the effect of poor electrical conductivity
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Embodiment 1
[0027] A method for preparing graphene-coated conductive fiber. The protein fiber is immersed in a positively charged graphene oxide dispersion at a temperature of 10°C. The pH of the protein fiber is> pI, the surface is negatively charged, and positively charged graphene oxide is adsorbed. After taking it out, it is rinsed and dried with deionized water, and then the graphene oxide on the fiber surface is reduced to graphene by a chemical reduction method to obtain a graphene-coated conductive fiber. Among them, the mass ratio of the negatively charged protein fibers on the surface to the positively charged graphene oxide dispersion is 1:100. The preparation method of the positively charged graphene oxide dispersion is as follows: the negatively charged concentration is 0.5 mg / mL Add 5mM AlCl to the graphene oxide dispersion 3 Solution to prepare a positively charged graphene oxide dispersion with a concentration of 0.1 mg / mL, a negatively charged graphene oxide dispersion and A...
Embodiment 2
[0030] A method for preparing graphene-coated conductive fiber. The modified negatively charged polyacrylonitrile fiber is immersed in a positively charged graphene oxide dispersion at a temperature of 15°C, and deionized water is taken out for rinsing and After drying, soaking in negatively charged graphene oxide dispersion liquid, taking it out, rinsing with deionized water and drying, reducing the graphene oxide on the fiber surface to graphene by high temperature thermal reduction method to obtain graphene coated conductive fiber. The mass ratio of the polyacrylonitrile fiber with negatively charged surface to the positively charged graphene oxide dispersion is 1:100, and the positively charged graphene oxide dispersion refers to the negatively charged concentration of 1.5mg / mL oxidation Add FeCl at a concentration of 0.1M to the graphene dispersion 3 The positively charged graphene oxide dispersion with the concentration of 0.5 mg / mL prepared in the solution, the negatively...
Embodiment 3
[0033] A method for preparing graphene-coated conductive fiber. The modified negatively charged PET fiber is immersed in a positively charged graphene oxide dispersion at a temperature of 20°C, and deionized water is taken out to rinse and dry. Then soak into the negatively charged graphene oxide dispersion, take it out, rinse and dry with deionized water, then soak again into the positively charged graphene oxide dispersion, take out the deionized water to rinse and dry, and finally remove it by UV Graphene oxide on the fiber surface is reduced to graphene to obtain graphene-coated conductive fiber. The mass ratio of the negatively charged PET fiber to the positively charged graphene oxide dispersion is 1:80, and the positively charged graphene oxide dispersion refers to graphite oxide with a concentration of 4.0 mg / mL that is negatively charged. 200mM TiCl was added to the ene dispersion 4 The positively charged graphene oxide dispersion with the concentration of 2.0 mg / mL pr...
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