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Preparation method and application in cigarettes of cigarette mango perfume

A mango and spice technology is applied in the field of preparation of mango spice for cigarettes, and achieves the effects of increasing sweetness, comfortable aftertaste, and reducing irritation and miscellaneous air.

Inactive Publication Date: 2018-11-23
CHINA TOBACCO GUANGXI IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is no use of membrane separation technology to separate mango extract to prepare tobacco flavor

Method used

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  • Preparation method and application in cigarettes of cigarette mango perfume
  • Preparation method and application in cigarettes of cigarette mango perfume
  • Preparation method and application in cigarettes of cigarette mango perfume

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Fresh ripe mangoes were taken, peeled, cut into uniform slices, placed in an oven, and dried at 50°C for 12 hours. Take the dried mango slices, pulverize them into coarse powder, and pass through a 10-mesh stainless steel sieve. Accurately weigh 100g of mango powder, wrap it with filter paper and put it into a Soxhlet extractor, add 500mL of 90% ethanol, heat at 80°C, and heat to reflux for 2h. Filter and distill the filtrate under reduced pressure until no ethanol flows out to obtain mango extract. Accurately weigh 10g of mango extract and place it in a 1000mL beaker, add 500mL of 20% ethanol to dissolve (N1). After the dissolution is complete, use a 50nm ceramic microfiltration membrane to filter, and the interception section is N2; the microfiltration membrane permeate is then filtered with a 100kd organic membrane, and the interception section is recorded as N3, and the permeation section is recorded as N4. Take the N3 part and distill it under reduced pressure to...

Embodiment 2

[0028] Fresh ripe mangoes were taken, peeled, cut into uniform slices, placed in an oven, and dried at 50°C for 12 hours. Take the dried mango slices, pulverize them into coarse powder, and pass through a 10-mesh stainless steel sieve. Accurately weigh 50g of mango powder, wrap it with filter paper and put it into a Soxhlet extractor, add 500mL of 50% ethanol, heat at 50°C, and heat to reflux for 2.5h. Filter and distill the filtrate under reduced pressure until no ethanol flows out to obtain mango extract. Accurately weigh 10g of mango extract and place it in a 1000mL beaker, add 500mL of 20% ethanol to dissolve (N1). After the dissolution is complete, use a 200nm ceramic microfiltration membrane to filter, and the interception section is N2; the microfiltration membrane permeate is then filtered with a 500kd organic membrane, and the interception section is recorded as N3, and the permeation section is recorded as N4. Take the N3 part and distill it under reduced pressure ...

Embodiment 3

[0030] Fresh ripe mangoes were taken, peeled, cut into uniform slices, placed in an oven, and dried at 50°C for 12 hours. Take the dried mango slices, pulverize them into coarse powder, and pass through a 10-mesh stainless steel sieve. Accurately weigh 150g of mango powder, wrap it with filter paper and put it into a Soxhlet extractor, add 450mL of 100% ethanol (absolute ethanol), heat at 90°C, and heat to reflux for 1h. Filter and distill the filtrate under reduced pressure until no ethanol flows out to obtain mango extract. Accurately weigh 10g of mango extract and place it in a 1000mL beaker, add 500mL of 20% ethanol to dissolve (N1). After the dissolution is complete, use a 100nm ceramic microfiltration membrane to filter, and the cut-off section is N2; the microfiltration membrane permeate is then filtered with a 10kd organic membrane, and the cut-off section is recorded as N3, and the permeated section is recorded as N4. Take the N3 part and distill it under reduced pr...

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Abstract

The invention provides a preparation method of cigarette mango perfume. The method comprises the steps that fresh and ripe mangoes are dried, pulverized and screened, ethanol heating and extracting and filtering are conducted, and concentration is conducted to obtain mango extract; ethanol dissolving is conducted on the mango extract, large molecular substances are removed by filtering using a ceramic microfiltration membrane, microfiltration membrane permeation liquid is filtered through an organic ultrafiltration membrane to remove part of small molecular substances influencing fragrance andtaste, part of the organic ultrafiltration membrane is reserved, and pressure reduction, distillation and concentration are conducted to obtain the mango perfume. The invention further discloses theapplication of the perfume in cigarettes, the cigarette mango perfume is diluted by using the organic solvent without toxin and irritating gas and sprayed on cut tobacco in a certain ratio, and the cut tobacco is rolled and produced into cigarettes. After adding the perfume, the fragrance amount can be obviously increased, fruit sweet fragrance is outstanding, the fragrance is harmony, sweet tasteis increased, irritation and impurity gas can be reduced, therefore smoking fume is gentle, and remaining smell is comfortable.

Description

technical field [0001] The invention belongs to the technical field of preparation of tobacco additives, and in particular relates to a preparation method of tobacco mango spice and its application in cigarettes. technical background [0002] As a fruit familiar to people, mango is rich in vitamins and amino acids. It is sweet and delicious, and the fresh fruit has a strong fragrance. Wei Changbin and others used headspace solid-phase microextraction to extract volatile components in mango, and carried out gas chromatography-mass spectrometry analysis and identification. The results showed that the volatile components in mango were mainly terpene compounds, such as α-terpinolene and δ-3-carene, and many of these volatile components were important components of natural flavors. There are few reports on the application of mango products in cigarette flavoring. [0003] Natural flavor components extracted by conventional extraction methods, such as Soxhlet extraction, inevita...

Claims

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Application Information

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IPC IPC(8): A24B3/12A24B15/24C11B9/02
CPCA24B3/12A24B15/241C11B9/022C11B9/025C11B9/027
Inventor 胡志忠宁振兴吴彦黄东业农李政刘鸿李志华杨龙彦徐石磊廖超执宋凌勇陈义昌胡超黄善松班强务文涛白家峰
Owner CHINA TOBACCO GUANGXI IND
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