Water-based polyketone-modified polyurethane emulsion for water-based gravure ink and its preparation method and application
A polyurethane emulsion and water-based polyurethane technology, applied in the field of water-based polyurethane, can solve the problems of no adhesion, no adhesion of BOPP film, etc., and achieve the effect of good water resistance, solving the environment and human body unfriendly, and excellent adhesion.
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Embodiment 1
[0031] (1) Preparation of water-based polyurethane emulsion:
[0032] Put 100g of hydroxyl-terminated polybutadiene (hydroxyl value: 101mgkoH / g), 45g of isophorone diisocyanate (IPDI) into a three-necked flask, heat up to 110°C for 1.5h, cool down to 80°C, and add 170g of butanone , then add 9g dimethylolpropionic acid (DMPA), 5g Yermer TM N120, react at 80°C for 3h, cool down to 30°C, add 18.8g of 20% by mass KOH ethanol solution, react for 15min, add 4g of 90% solid content of sodium diaminesulfonate aqueous solution (PPS) for 30min, and then Add 318g of pure water and stir at high speed to form a stable homogeneous liquid, then add 5g of isophorone diamine (IPD), react for 45min, heat up to 50-80°C, remove methyl ethyl ketone in a vacuum, and obtain a water-based solution with a solid content of 35%. Polyurethane semipermeable emulsion.
[0033] (2) Preparation of water-based polyketone emulsion:
[0034] Get 200g mass fraction and be the anhydrous methyl ethyl ketone s...
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