Aqueous pressure-sensitive adhesive for heat-insulating broken bridge aluminum profile protection film and preparation method thereof
A technology for thermal insulation, bridge breaking and protective film, applied in pressure-sensitive films/sheets, adhesive types, ester copolymer adhesives, etc., to improve cohesive strength, improve heat and moisture resistance, and improve adhesion Effect
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Embodiment 1
[0032] A water-based acrylic pressure-sensitive adhesive for the protective film of heat-insulating bridge-breaking aluminum profiles, the preparation steps of which are as follows:
[0033] 1. Preparation of seed emulsion: Mix 34 parts of deionized water and 2.0 parts of allyloxynonylphenol polyoxyethylene ether ammonium sulfate, stir evenly at a stirring speed of 500 rpm, and then slowly mix 5 parts of Methyl methacrylate, 45 parts of 2-ethylhexyl acrylate, 45 parts of butyl acrylate, 2 parts of N-methylolacrylamide, 3 parts of hydroxyethyl acrylate, 0.1 part of n-dodecane Add mercaptan dropwise and stir for 20-30 minutes to obtain pre-emulsion I; mix 82 parts of deionized water, 0.3 parts of allyloxynonylphenol polyoxyethylene ether ammonium sulfate, and put 5 parts of pre-emulsion I into In the reaction kettle, start to heat up to 85°C, then add 0.1 parts of initiator to the system, initiate the polymerization of the system, and react for 30 minutes; then dropwise add the ...
Embodiment 2
[0038] A water-based acrylic pressure-sensitive adhesive for the protective film of heat-insulating bridge-breaking aluminum profiles, the preparation steps of which are as follows:
[0039] 1. Preparation of seed emulsion: Mix 34 parts of deionized water and 2.0 parts of allyloxynonylphenol polyoxyethylene ether ammonium sulfate, stir evenly at a stirring speed of 500 rpm, and then slowly mix 5 parts of Methyl methacrylate, 45 parts of 2-ethylhexyl acrylate, 45 parts of butyl acrylate, 2 parts of N-methylolacrylamide, 3 parts of hydroxyethyl acrylate, 0.1 part of n-dodecane Add mercaptan dropwise and stir for 20-30 minutes to obtain pre-emulsion I; mix 82 parts of deionized water, 0.3 parts of allyloxynonylphenol polyoxyethylene ether ammonium sulfate, and put 7 parts of pre-emulsion I into In the reaction kettle, start to heat up to 85°C, then add 0.1 parts of initiator to the system, initiate the polymerization of the system, and react for 30 minutes; then dropwise add the ...
Embodiment 3
[0044] A water-based acrylic pressure-sensitive adhesive for the protective film of heat-insulating bridge-breaking aluminum profiles, the preparation steps of which are as follows:
[0045] 1. Preparation of seed emulsion: Mix 34 parts of deionized water and 2.0 parts of allyloxynonylphenol polyoxyethylene ether ammonium sulfate, stir evenly at a stirring speed of 500 rpm, and then slowly mix 5 parts of Methyl methacrylate, 45 parts of 2-ethylhexyl acrylate, 45 parts of butyl acrylate, 2 parts of N-methylolacrylamide, 3 parts of hydroxyethyl acrylate, 0.1 part of n-dodecane Add mercaptan dropwise and stir for 20-30 minutes to obtain pre-emulsion I; mix 82 parts of deionized water, 0.3 parts of allyloxynonylphenol polyoxyethylene ether ammonium sulfate, and put 7 parts of pre-emulsion I into In the reaction kettle, start to heat up to 85°C, then add 0.1 parts of initiator to the system, initiate the polymerization of the system, and react for 30 minutes; then dropwise add the ...
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