Preparation method of large-area non-laminated structure NiSe nano-film
A non-layered structure, nano-thin film technology, applied in the direction of nanotechnology, coating, metal material coating technology, etc., can solve the problem of high cost, achieve the effect of good quality, small number of grain boundaries, and simple preparation process
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[0013] The following description serves to disclose the present invention to enable those skilled in the art to carry out the present invention. The preferred embodiments described below are only examples, and those skilled in the art can devise other obvious variations.
[0014] The present invention will be further described below in conjunction with the examples, but the protection scope of the present invention is not limited only to the examples.
[0015] A method for preparing a large-area non-layered structure NiSe nano film, comprising the following steps:
[0016] (1) Preparation of NiSe nano-film: Ni foil with a thickness of 50 μm and a purity of 99.99% was annealed at 500 °C for 30 min in a low-pressure atmosphere with 10 sccm H2 and 20 sccm Ar to remove the oxides on the surface of the Ni foil ; After annealing, use electron beam evaporation method to deposit ZnSe thin film on the surface of Ni foil. During the whole deposition process, the vacuum degree is kept a...
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