Condensation recovery process of pentadiene in production of methyl tetrahydrophthalic anhydride
A methyltetrahydrophthalic anhydride, condensation recovery technology, applied in the direction of hydrocarbons, hydrocarbon purification/separation, chemical instruments and methods, etc., can solve the problem that the boiling point of pentadiene is low enough to recover pentadiene , waste of pentadiene raw materials and other issues, to achieve the effects of low content of harmful substances, increase energy utilization rate, and protect the environment
Inactive Publication Date: 2019-01-04
嘉兴南洋万事兴化工有限公司
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[0004] The above-mentioned prior art scheme has the following defects: due to the low boiling point of pentadiene, it is not enough to recover most of the pentadiene through the above-mentioned condensation operation, and a considerable part of pentadiene exists in the tail gas, resulting in the production of pentadiene raw materials. waste of
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Embodiment 1
[0042] Embodiment 10, a pentadiene condensation recovery process in the production of methyltetrahydrophthalic anhydride, differs from Example 1 in that the coolant is ethylene glycol C 2 h 6 o 2 .
Embodiment 11
[0043] Example 11, a pentadiene condensation recovery process in the production of methyltetrahydrophthalic anhydride, differs from Example 1 in that the alcohol or salt coolant is magnesium chloride MgCl 2 .
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Abstract
The invention relates to a condensation recovery process of pentadiene in the production of methyl tetrahydrophthalic anhydride, and belongs to the technical field of gas condensation recovery. The technical key points include: step A, pentadiene steam passes through a primary condenser, a coolant is circulating water, liquid pentadiene enters a recovery tank from the bottom of the condenser, andthe residual gas is discharged from the upper end of the condenser; step B, the residual gas enters a secondary condenser, the coolant is a salt and alcohol solution, liquid pentadiene enters the recovery tank from the bottom of the condenser, and the residual gas is discharged from the upper end of the condenser; and step C, the residual gas is pressurized and then enters a tertiary condenser, liquid pentadiene enters the recovery tank from the bottom of the condenser, and the residual gas enters a tail gas treatment device. The condensation recovery process of pentadiene in the production ofmethyl tetrahydrophthalic anhydride has the advantages of simple operation, improved pentadiene recovery rate through multistage condensation, and improved energy utilization rate through heat exchange between material flows.
Description
technical field [0001] The invention relates to the technical field of gas condensation recovery, in particular to a pentadiene condensation recovery process in the production of methyltetrahydrophthalic anhydride. Background technique [0002] At present, methyltetrahydrophthalic anhydride has the characteristics of low viscosity, stable performance, low freezing point, long pot life, low volatility, low toxicity, and good mutual solubility. Therefore, it is an indispensable new fine chemical product for electronic industry and electromechanical industry products. Widely used in potting, casting, encapsulation, lamination, molding, bonding, winding and other processes. Pentadiene is an important raw material for the production of methyltetrahydrophthalic anhydride. Pentadiene mainly comes from the coking industry. Due to the lack of oil cracking and recovery industries, the output is very small and the supply exceeds demand. [0003] The existing technology for the conde...
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IPC IPC(8): C07C11/173C07C7/04
CPCC07C7/005C07C7/04C07C11/173
Inventor 王海斌
Owner 嘉兴南洋万事兴化工有限公司
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