aln and mgb 2 Particle reinforced magnesium matrix composite material and preparation method thereof
A composite material and particle reinforcement technology, applied in the field of metal matrix composite materials, can solve the problems of difficult control of the reaction process, unsuitable for large-scale production, complex preparation process, etc., and achieve the effects of thermodynamic stability, clean surface and no pollution, and high bonding strength.
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Embodiment 1
[0019] (1) First prepare the required raw materials according to the following mass percentages: industrial pure magnesium powder 90.7 (size ≤ 30 μm), industrial pure aluminum powder 6.2 (size ≤ 30 μm), boron nitride powder 3.0 (size ≤ 1 μm), graphene 0.1 ;
[0020] (2) Take the material in the step (1) in proportion, at first magnesium powder and aluminum powder are ball milled at low speed (ball mill speed 120r / min) 16h, then it is high-speed ball milled together with boron nitride powder and graphene (ball mill speed 400r / min) for 0.5h, the above two steps of ball milling are all carried out under an argon atmosphere, and the ball-to-material ratio is set at 4:1;
[0021] (3) degassing the material after the two-step ball milling in step (2), and pressing it into a prefabricated body in a cold isostatic press;
[0022] (4) Put the prefabricated body into the vacuum sintering furnace, set the vacuum degree at 6×10 -3 Pa, control the sintering temperature to 480°C, and the ...
Embodiment 2
[0025] (1) First prepare the required raw materials according to the following mass percentages: industrial pure magnesium powder 73.0 (size ≤ 40 μm), industrial pure aluminum powder 16.8 (size ≤ 50 μm), boron nitride powder 10.0 (size ≤ 1 μm), graphene 0.2 ;
[0026] (2) Take the material in the step (1) in proportion, at first magnesium powder and aluminum powder are ball milled at low speed (ball mill speed 100r / min) 24h, then it is ball milled at high speed (ball mill speed 100r / min) together with boron nitride powder and graphene 480r / min) 2h, the above two steps of ball milling are all carried out under argon atmosphere, and the ball-to-material ratio is set at 5:1;
[0027] (3) degassing the material after the two-step ball milling in step (2), and pressing it into a prefabricated body in a hot isostatic press;
[0028] (4) Put the prefabricated body into the vacuum sintering furnace, set the vacuum degree at 7×10 -3 Pa, the sintering temperature is controlled to be 5...
Embodiment 3
[0031] (1) First prepare the required raw materials according to the following mass percentages: industrial pure magnesium powder 59.5 (size ≤ 60 μm), industrial pure aluminum powder 25.2 (size ≤ 70 μm), boron nitride powder 15.0 (size ≤ 2 μm), graphene 0.3 ;
[0032] (2) Take the material in step (1) in proportion, at first magnesium powder and aluminum powder are ball milled at low speed (ball mill speed 120r / min) 36h, then it is high-speed ball milled together with boron nitride powder and graphene (ball mill speed 400r / min) 6h, the above two steps of ball milling are all carried out under argon atmosphere, and the ball-to-material ratio is set at 6:1;
[0033] (3) degassing the material after the two-step ball milling in step (2), and pressing it into a prefabricated body in a cold isostatic press;
[0034] (4) Put the prefabricated body into the vacuum sintering furnace, set the vacuum degree at 9×10 -3Pa, control the sintering temperature to 650°C, and the holding time...
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