Polishing pad, manufacturing method of polishing pad, and polishing method
A manufacturing method and technology of grinding pads, which are applied in the fields of grinding tools, semiconductor/solid-state device manufacturing, electrical components, etc., can solve problems that have not yet been discovered, and achieve the effect of excellent grinding rate
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[0112] Hereinafter, the present invention will be specifically described by way of examples and comparative examples.
Synthetic example 1
[0113] (Synthesis Example 1: Synthesis of Urethane Prepolymer (A1))
[0114] 2,366 parts by mass of toluene diisocyanate (TDI-80) were charged into a 5-liter four-necked round-bottomed flask equipped with a nitrogen gas introduction pipe, a condenser for cooling, a thermometer, and a stirrer, and stirring was started. Next, 2,028 parts of polytetramethylene glycol (number average molecular weight: 1,000) was charged and mixed, and reacted at 80° C. for 3 hours under a nitrogen atmosphere. Next, 15 parts by mass of a polysiloxane compound (manufactured by Shin-Etsu Chemical Co., Ltd., "X-22-176DX"; single-end silicone diol, number average molecular weight: 3262) was charged and mixed, and heated at 80°C under a nitrogen stream. The reaction was carried out for 3 hours. Next, 591 parts by mass of diethylene glycol was reacted for 3 hours while paying attention to heat generation, and an isocyanate group-terminated urethane prepolymer (A1) having an NCO equivalent of 420 was obt...
Synthetic example 2
[0115] (Synthesis Example 2: Synthesis of Urethane Prepolymer (A2))
[0116] 2,366 parts by mass of toluene diisocyanate (TDI-80) were charged into a 5-liter four-necked round-bottomed flask equipped with a nitrogen gas introduction pipe, a condenser for cooling, a thermometer, and a stirrer, and stirring was started. Next, 2,044 parts by mass of polytetramethylene glycol (number average molecular weight: 1,000) was charged and mixed, and reacted at 80° C. for 3 hours under a nitrogen stream. Next, 590 parts by mass of diethylene glycol was reacted for 3 hours while paying attention to heat generation, and an isocyanate group-terminated urethane prepolymer (A2) having an NCO equivalent of 420 was obtained.
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