Crocin standard product prepared from fructus gardeniae by utilizing novel filler and preparation method thereof
A technology of saffron and standard products, applied in the field of bioengineering, can solve the problems of long production cycle, unsuitable for industrial production, cumbersome process, etc., and achieve the effects of low cost, easy industrial production, and simple process flow
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
preparation example Construction
[0044] The first embodiment of the present invention provides a method for preparing a novel filler, which specifically includes the following steps:
[0045] 1. Prepare monomer: put 120-130kg styrene (cross-linking monomer), 9-10kg methyl acrylate (monomer) and 1-1.5kg dibenzoyl peroxide (catalyst) into No. 1 reactor, Mix and stir at room temperature for 25 to 30 minutes, then add 170 to 180 kg of methylcyclohexane (porogen), and stir at room temperature for 25 to 30 minutes to obtain monomers;
[0046] 2. Preparation of water phase: Put appropriate amount of water in No. 2 reactor, then put in powdered salt, stir to make the brine uniform, the specific gravity of the brine is 1.12-1.2, put 7-9kg of gelatin and 0.01- 0.03kg of methylene blue, stir and heat to 55-60°C, stop stirring and keep warm to obtain the water phase;
[0047] 3. Pump the prepared monomer from the No. 1 reactor into the No. 2 reactor, and directly start stirring for 10-15 minutes without heating up to ob...
Embodiment 1
[0075] 1. Put 120kg of styrene, 9kg of methyl acrylate and 1kg of dibenzoyl peroxide into the No. 1 reactor, mix and stir at room temperature for 30 minutes, then add 170kg of methylcyclohexane, and stir at room temperature for 25 minutes to obtain the monomer;
[0076] 2. Put brine with a specific gravity of 1.12, 9kg of gelatin and 0.01kg of methylene blue into the No. 2 reactor, stir and heat to 55°C, stop stirring and keep warm to obtain the water phase;
[0077] 3. Pump the monomer from the No. 1 reactor into the No. 2 reactor, and directly start stirring for 10 minutes without heating up to obtain the mixed material. Slowly raise the temperature of the mixed material in the No. 2 reactor to 68 ° C and keep it warm for 4 hours Finally, the steam heating slowly raises the temperature to 70°C, and keeps the temperature for 6 hours. The stirring cannot be stopped during the whole process. The mixed material is gradually formed into a new type of spherical particle filler duri...
Embodiment 2
[0096] 1. Put 125kg styrene, 9.5kg methyl acrylate and 1.2kg dibenzoyl peroxide into No. 1 reactor, mix and stir at room temperature for 28min, then drop into 172kg methylcyclohexane, stir at room temperature for 26min to obtain a single body;
[0097] 2. Put brine with a specific gravity of 1.15, 8.5kg of gelatin and 0.02kg of methylene blue into the No. 2 reactor, stir and heat to 60°C, stop stirring and keep warm to obtain the water phase;
[0098] 3. Pump the monomer from the No. 1 reactor into the No. 2 reactor, and directly start stirring for 10 minutes without heating up to obtain the mixed material. Slowly raise the temperature of the mixed material in the No. 2 reactor to 70°C and keep it warm for 5 hours Finally, the steam heating slowly raises the temperature to 75°C, and keeps the temperature for 6.5 hours. The stirring cannot be stopped during the whole process. The mixed material is gradually formed into a new type of spherical particle filler during the above-me...
PUM
| Property | Measurement | Unit |
|---|---|---|
| height | aaaaa | aaaaa |
| height | aaaaa | aaaaa |
| height | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More