Single-component silane-modified polyether sealant and production method and application thereof

A silane-modified polyether and sealant technology, which is applied in the field of construction sealants, can solve the problems of base material pollution and poor weather resistance, and achieve the effects of good adhesion, excellent weather resistance and good elasticity

Inactive Publication Date: 2019-06-07
GUANGZHOU GLORYSTAR CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Based on this, it is necessary to provide a one-component silane-modified polyether sealant for the poor wea...

Method used

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  • Single-component silane-modified polyether sealant and production method and application thereof
  • Single-component silane-modified polyether sealant and production method and application thereof
  • Single-component silane-modified polyether sealant and production method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] A preparation method of a one-component silane-modified polyether sealant, comprising the following steps:

[0039] Step 1: Mix 30 parts of STP-E30, 10 parts of cyclohexane 1,2-diisononyl dicarboxylate, 20 parts of heavy calcium carbonate, 30 parts of nano calcium carbonate, 4 parts of titanium dioxide, 0.25 parts of UV326, 0.25 Add UV770 and 0.25 Irganox1010 into the stirring tank, stir in vacuum for 5 minutes, heat up to 100-110°C and stir in vacuum for 2 hours to dehydrate;

[0040] Step 2: Cool down to 80-85°C, add 2 parts of polyamide wax, vacuumize and stir for 30 minutes, and the stirring speed is 800rpm;

[0041] Step 3: Cool down to below 50°C under vacuum protection, add 1 part of vinyltrimethoxysilane, 0.6 part of N-β-(aminoethyl)-γ-aminopropyltrimethoxysilane, 0.4 part of γ-shrink Glyceryl ether oxypropyltrimethoxysilane, 0.3 parts of modified organotin compounds, and vacuum stirring for 30 minutes to obtain a one-component silane-modified polyether sealant...

Embodiment 2

[0043] A preparation method of a one-component silane-modified polyether sealant, comprising the following steps:

[0044] Step 1: Mix 10 parts of STP-E10, 15 parts of STP-E35, 15 parts of diisononyl phthalate, 23 parts of heavy calcium carbonate, 30 parts of nano calcium carbonate, 2 parts of carbon black, 0.20 parts of UV327, 0.3 Add 1 part of Tinuvin 123 and 0.20 part of Irganox 245 into the stirred tank, stir in vacuum for 5 minutes, heat up to 100-110°C and stir in vacuum for 2 hours to dehydrate;

[0045] Step 2: Cool down to 80-85°C, add 2 parts of polyamide wax, vacuumize and stir for 30 minutes, and the stirring speed is 800rpm;

[0046] Step 3: Reduce the temperature to below 50°C under vacuum protection, add 1 part of vinyltrimethoxysilane, 0.6 parts of γ-aminopropyltrimethoxysilane, 0.4 parts of γ-glycidyl etheroxypropyltrimethoxysilane, 0.3 parts of modified organotin compounds were stirred in vacuum for 30 minutes to obtain a one-component silane-modified polyethe...

Embodiment 3

[0048] A preparation method of a one-component silane-modified polyether sealant, comprising the following steps:

[0049] Step 1: Add 30 parts of STP-E30, 20 parts of STP-E15, 35 parts of nano calcium carbonate, 10 parts of heavy calcium carbonate, 3 parts of carbon black, 0.3 parts of UV326, 0.2 parts of Tinuvin123, 0.3 parts of Irganox1076 into the stirring tank , stir in vacuum for 5 minutes, heat up to 100-110°C and stir in vacuum for 2 hours to dehydrate;

[0050] Step 2: Cool down to 80-85°C, add 1 part of polyamide wax, vacuumize and stir for 30 minutes, and the stirring speed is 700rpm;

[0051] Step 3: Cool down to below 50°C under vacuum protection, add 1 part of vinyltrimethoxysilane, 0.7 part of γ-aminopropyltrimethoxysilane, 0.3 part of γ-glycidyl etheroxypropyltrimethoxysilane, 0.4 parts of modified organotin compounds were stirred in vacuum for 30 minutes to obtain a one-component silane-modified polyether sealant.

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PUM

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Abstract

The invention provides a single-component silane-modified polyether sealant and a production method and application thereof, and belongs to the field of building sealants. The sealant comprises the following raw materials of, in parts by weight, 20-50 parts of silane-modified polyether resin, 0-15 parts of plasticizer, 30-60 parts of filler, 1-2 parts of thixotropic agent, 0.4-1.5 parts of functional assistant, 0.5-2 parts of moisture scavenger, 0.5-2 parts of bonding accelerator and 0.05-0.5 part of catalyst. The sealant is excellent in weather resistance performance, the phenomena of cracking and efflorescence are not liable to occur, and no pollution is caused for a stone curtain wall.

Description

technical field [0001] The invention relates to the field of building sealants, in particular to a one-component silane-modified polyether sealant and its preparation method and application. Background technique [0002] Sealant is a material used to fill gaps. It is a fluid or paste-like amorphous material during construction. After construction, it relies on solvent volatilization or chemical reaction to bond with the substrate to play the role of bonding, fixing and sealing. . Silane-modified polyether sealant, because it combines the advantages and strengths of silicone sealant and polyurethane sealant, has excellent durability, high resistance to deformation and displacement, good adhesion, paintability, and environmental friendliness The advantages of non-toxicity, low staining, low viscosity and good workability have attracted more and more attention from the domestic construction industry. [0003] The traditional stone curtain wall caulking glue is mainly silicone...

Claims

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Application Information

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IPC IPC(8): C09J171/00C09J11/04C09J11/06C09J11/08
Inventor 曾军程小莲张少鸿吴锦龙
Owner GUANGZHOU GLORYSTAR CHEM
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